3-(3-chlorophenyl) 4-(5-iodo-2-benzimidazolyl)butanoic acid hydrochloride

Base Information

Chemical Name:3-(3-chlorophenyl) 4-(5-iodo-2-benzimidazolyl)butanoic acid hydrochloride
CAS No.:1221962-36-2
Molecular Formula:C₁₇H₁₄ClIN₂O₂*ClH
Molecular Weight:477.129
Hs Code.:

Synonyms:3-(3-chlorophenyl) 4-(5-iodo-2-benzimidazolyl)butanoic acid hydrochloride

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Chemical Property of 3-(3-chlorophenyl) 4-(5-iodo-2-benzimidazolyl)butanoic acid hydrochloride

Chemical Property:

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Technology Process of 3-(3-chlorophenyl) 4-(5-iodo-2-benzimidazolyl)butanoic acid hydrochloride

There total 7 articles about 3-(3-chlorophenyl) 4-(5-iodo-2-benzimidazolyl)butanoic acid hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20691-72-9
4-iodo-2-nitroaniline

: 1221962-36-2
3-(3-chlorophenyl) 4-(5-iodo-2-benzimidazolyl)butanoic acid hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: tin(II) chloride dihdyrate / ethanol / 2 h / 75 °C

2: tetrahydrofuran / 1 h / 20 °C

3: hydrogenchloride; acetic acid / water / 3 h / Reflux

With hydrogenchloride; tin(II) chloride dihdyrate; acetic acid; In tetrahydrofuran; ethanol; water;
DOI:10.1021/jm2005892

Reference yield:

: C₁₇H₁₆ClIN₂O₃

: 1221962-36-2
3-(3-chlorophenyl) 4-(5-iodo-2-benzimidazolyl)butanoic acid hydrochloride

Guidance literature:: With hydrogenchloride; acetic acid; In water; for 3h; Reflux;
DOI:10.1021/jm2005892

Reference yield:

: 4759-58-4
acide (chloro-3 phenyl)-3 glutarique

: 1221962-36-2
3-(3-chlorophenyl) 4-(5-iodo-2-benzimidazolyl)butanoic acid hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: acetyl chloride / 2 h / Reflux

2: tetrahydrofuran / 1 h / 20 °C

3: hydrogenchloride; acetic acid / water / 3 h / Reflux

With hydrogenchloride; acetic acid; acetyl chloride; In tetrahydrofuran; water;
DOI:10.1021/jm2005892