cyclo[-N-methyl-L-leucinyl-D-(hydroxyimino)lactyl-N-methyl-L-leucinyl-D-phenyllactyl-N-methyl-L-leucinyl-D-lactyl-N-methyl-L-leucinyl-D-phenyllactyl-]

Base Information

• Chemical Name: cyclo[-N-methyl-L-leucinyl-D-(hydroxyimino)lactyl-N-methyl-L-leucinyl-D-phenyllactyl-N-methyl-L-leucinyl-D-lactyl-N-methyl-L-leucinyl-D-phenyllactyl-]
• CAS No.: 496808-84-5
• Molecular Formula: C₅₂H₇₇N₅O₁₂
• Molecular Weight: 964.21

Synonyms:cyclo[-N-methyl-L-leucinyl-D-(hydroxyimino)lactyl-N-methyl-L-leucinyl-D-phenyllactyl-N-methyl-L-leucinyl-D-lactyl-N-methyl-L-leucinyl-D-phenyllactyl-]

Chemical Property of cyclo[-N-methyl-L-leucinyl-D-(hydroxyimino)lactyl-N-methyl-L-leucinyl-D-phenyllactyl-N-methyl-L-leucinyl-D-lactyl-N-methyl-L-leucinyl-D-phenyllactyl-]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of cyclo[-N-methyl-L-leucinyl-D-(hydroxyimino)lactyl-N-methyl-L-leucinyl-D-phenyllactyl-N-methyl-L-leucinyl-D-lactyl-N-methyl-L-leucinyl-D-phenyllactyl-]

There total 2 articles about cyclo[-N-methyl-L-leucinyl-D-(hydroxyimino)lactyl-N-methyl-L-leucinyl-D-phenyllactyl-N-methyl-L-leucinyl-D-lactyl-N-methyl-L-leucinyl-D-phenyllactyl-] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

cyclo[-N-methyl-L-leucinyl-D-(benzyloxyimino)lactyl-N-methyl-L-leucinyl-D-phenyllactyl-N-methyl-L-leucinyl-D-lactyl-N-methyl-L-leucinyl-D-phenyllactyl-] → cyclo[-N-methyl-L-leucinyl-D-(hydroxyimino)lactyl-N-methyl-L-leucinyl-D-phenyllactyl-N-methyl-L-leucinyl-D-lactyl-N-methyl-L-leucinyl-D-phenyllactyl-] (496808-84-5)

Guidance literature:

With hydrogenchloride; 10% palladium on active carbon; hydrogen; In methanol; at 20 ℃; for 0.333333h;

DOI:10.1002/ps.590

Reference yield:

(3S,6R,9S,12R,15S,18R,21S,24R)-6,18-Dibenzyl-3,9,15,21-tetraisobutyl-4,10,12,16,22,24-hexamethyl-23-thioxo-1,7,13,19-tetraoxa-4,10,16,22-tetraaza-cyclotetracosane-2,5,8,11,14,17,20-heptaone → cyclo[-N-methyl-L-leucinyl-D-(hydroxyimino)lactyl-N-methyl-L-leucinyl-D-phenyllactyl-N-methyl-L-leucinyl-D-lactyl-N-methyl-L-leucinyl-D-phenyllactyl-] (496808-84-5)

Guidance literature:

With mercury(II) diacetate; hydroxylamine; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃;

DOI:10.1002/ps.590

Reference yield: 80.0%

chloroformic acid ethyl ester (541-41-3) + cyclo[-N-methyl-L-leucinyl-D-(hydroxyimino)lactyl-N-methyl-L-leucinyl-D-phenyllactyl-N-methyl-L-leucinyl-D-lactyl-N-methyl-L-leucinyl-D-phenyllactyl-] (496808-84-5) → cyclo[-N-methyl-L-leucinyl-D-(ethoxycarbonyloxyimino)lactyl-N-methyl-L-leucinyl-D-phenyllactyl-N-methyl-L-leucinyl-D-lactyl-N-methyl-L-leucinyl-D-phenyllactyl-]

Guidance literature:

In pyridine; at 0 ℃; for 6h;

DOI:10.1002/ps.590

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