N-(4-aminobutyl)-N, N',N''-tris(2-pyridylmethyl)-cis,cis-1,3,5-triaminocyclohexane

Base Information

Chemical Name:N-(4-aminobutyl)-N, N',N''-tris(2-pyridylmethyl)-cis,cis-1,3,5-triaminocyclohexane
CAS No.:479251-96-2
Molecular Formula:C₂₈H₃₉N₇
Molecular Weight:473.665
Hs Code.:

Synonyms:N-(4-aminobutyl)-N, N',N''-tris(2-pyridylmethyl)-cis,cis-1,3,5-triaminocyclohexane

Suppliers and Price of N-(4-aminobutyl)-N, N',N''-tris(2-pyridylmethyl)-cis,cis-1,3,5-triaminocyclohexane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(4-aminobutyl)-N, N',N''-tris(2-pyridylmethyl)-cis,cis-1,3,5-triaminocyclohexane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(4-aminobutyl)-N, N',N''-tris(2-pyridylmethyl)-cis,cis-1,3,5-triaminocyclohexane

There total 9 articles about N-(4-aminobutyl)-N, N',N''-tris(2-pyridylmethyl)-cis,cis-1,3,5-triaminocyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 479251-95-1
2-[4-({(1S,3R,5S)-3,5-Bis-[(pyridin-2-ylmethyl)-amino]-cyclohexyl}-pyridin-2-ylmethyl-amino)-butyl]-isoindole-1,3-dione

: 479251-96-2
N-(4-aminobutyl)-N, N',N''-tris(2-pyridylmethyl)-cis,cis-1,3,5-triaminocyclohexane

Guidance literature:: With hydrogenchloride; for 5h; Heating;
DOI:10.1021/jo0204911

Reference yield:

: 1121-60-4
pyridine-2-carbaldehyde

: 479251-96-2
N-(4-aminobutyl)-N, N',N''-tris(2-pyridylmethyl)-cis,cis-1,3,5-triaminocyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: benzene / 7 h / Heating

2: 537 mg / NaBH₄ / ethanol / 24 h / 20 °C

3: 75 percent / aq. HCl / 5 h / Heating

With hydrogenchloride; sodium tetrahydroborate; In ethanol; benzene;
DOI:10.1021/jo0204911

Reference yield:

: 26150-46-9
cis,cis-1,3,5-triaminocyclohexane

: 479251-96-2
N-(4-aminobutyl)-N, N',N''-tris(2-pyridylmethyl)-cis,cis-1,3,5-triaminocyclohexane

Guidance literature:: Multi-step reaction with 8 steps

1: 52 percent / CHCl₃ / 2 h / Heating

2: benzene / 7 h / Heating

3: 656 mg / NaBH₄ / ethanol / 24 h / 20 °C

4: 81 percent / K₂CO₃ / acetonitrile / 36 h / Heating

5: 56 percent / CF₃CO₂H / CHCl₃; methanol / 48 h / -5 - 20 °C

6: benzene / 7 h / Heating

7: 537 mg / NaBH₄ / ethanol / 24 h / 20 °C

8: 75 percent / aq. HCl / 5 h / Heating

With hydrogenchloride; sodium tetrahydroborate; potassium carbonate; trifluoroacetic acid; In methanol; ethanol; chloroform; acetonitrile; benzene;
DOI:10.1021/jo0204911