(2E,8E)-10-(tert-Butyl-diphenyl-silanyloxy)-2,8-dimethyl-deca-2,8-dien-1-ol

Base Information

Chemical Name:(2E,8E)-10-(tert-Butyl-diphenyl-silanyloxy)-2,8-dimethyl-deca-2,8-dien-1-ol
CAS No.:882165-38-0
Molecular Formula:C₂₈H₄₀O₂Si
Molecular Weight:436.71
Hs Code.:

Synonyms:(2E,8E)-10-(tert-Butyl-diphenyl-silanyloxy)-2,8-dimethyl-deca-2,8-dien-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2E,8E)-10-(tert-Butyl-diphenyl-silanyloxy)-2,8-dimethyl-deca-2,8-dien-1-ol

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Technology Process of (2E,8E)-10-(tert-Butyl-diphenyl-silanyloxy)-2,8-dimethyl-deca-2,8-dien-1-ol

There total 9 articles about (2E,8E)-10-(tert-Butyl-diphenyl-silanyloxy)-2,8-dimethyl-deca-2,8-dien-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 882165-12-0
(2E,8E)-10-(tert-Butyl-diphenyl-silanyloxy)-2,8-dimethyl-deca-2,8-dienoic acid methyl ester

: 882165-38-0
(2E,8E)-10-(tert-Butyl-diphenyl-silanyloxy)-2,8-dimethyl-deca-2,8-dien-1-ol

Guidance literature:: With diisobutylaluminium hydride; In toluene; at -78 ℃; for 3h;
DOI:10.1021/ol060221v

Reference yield:

: 882165-43-7
8-(tert-butyl-diphenyl-silanyloxy)-6-methyl-oct-6-enal

: 882165-38-0
(2E,8E)-10-(tert-Butyl-diphenyl-silanyloxy)-2,8-dimethyl-deca-2,8-dien-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / toluene / 4 h / 80 °C

2: 92 percent / DIBALH / toluene / 3 h / -78 °C

With diisobutylaluminium hydride; In toluene;
DOI:10.1021/ol060221v

Reference yield:

: 882165-41-5
(2E,6E)-8-(tert-Butyl-diphenyl-silanyloxy)-6-methyl-octa-2,6-dienoic acid methyl ester

: 882165-38-0
(2E,8E)-10-(tert-Butyl-diphenyl-silanyloxy)-2,8-dimethyl-deca-2,8-dien-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 68 percent / BiCl₅; NaBH₄ / 4 h / 20 °C

2: 82 percent / DIBALH / toluene / 3 h / -78 °C

3: 85 percent / toluene / 4 h / 80 °C

4: 92 percent / DIBALH / toluene / 3 h / -78 °C

With sodium tetrahydroborate; bismuth (V) chloride; diisobutylaluminium hydride; In toluene;
DOI:10.1021/ol060221v