5-<1-(methoxyimino)ethyl>-2-phenyl<1,3,5>triazino<1,2-a>indole-1,3(2H,4H)-dione

Base Information

• Chemical Name: 5-<1-(methoxyimino)ethyl>-2-phenyl<1,3,5>triazino<1,2-a>indole-1,3(2H,4H)-dione
• CAS No.: 155794-85-7
• Molecular Formula: C₁₉H₁₆N₄O₃
• Molecular Weight: 348.361

Synonyms:5-<1-(methoxyimino)ethyl>-2-phenyl<1,3,5>triazino<1,2-a>indole-1,3(2H,4H)-dione

Chemical Property of 5-<1-(methoxyimino)ethyl>-2-phenyl<1,3,5>triazino<1,2-a>indole-1,3(2H,4H)-dione

Chemical Property:

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Technology Process of 5-<1-(methoxyimino)ethyl>-2-phenyl<1,3,5>triazino<1,2-a>indole-1,3(2H,4H)-dione

There total 1 articles about 5-<1-(methoxyimino)ethyl>-2-phenyl<1,3,5>triazino<1,2-a>indole-1,3(2H,4H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

5-<1-(methoxyimino)ethyl>-2-phenyl-1H-<1,2,4>triazolo<1,2-a>cinnoline-1,3(2H)-dione → 5-<1-(methoxyimino)ethyl>-2-phenyl<1,3,5>triazino<1,2-a>indole-1,3(2H,4H)-dione (155794-85-7)

Guidance literature:

In benzene; for 8h; Irradiation;

DOI:10.1246/cl.1994.771

Reference yield:

5-<1-(methoxyimino)ethyl>-2-phenyl<1,3,5>triazino<1,2-a>indole-1,3(2H,4H)-dione (155794-85-7) + methyl iodide (74-88-4) → 5-<1-(methoxyimino)ethyl>-4-methyl-2-phenyl<1,3,5>triazino<1,2-a>indole-1,3(2H,4H)-dione

Guidance literature:

With sodium hydroxide; tetrabutylammomium bromide; In dichloromethane;

DOI:10.1246/cl.1994.771

Reference yield:

5-<1-(methoxyimino)ethyl>-2-phenyl<1,3,5>triazino<1,2-a>indole-1,3(2H,4H)-dione (155794-85-7) + 9-methoxy-5-<1-(methoxyimino)ethyl>-2-phenyl-1H-<1,2,4>triazolo<1,2-a>cinnoline-1,3(2H)-dione (155794-84-6) → 8-methoxy-5-<1-(methoxyimino)ethyl>-2-phenyl<1,3,5>triazino<1,2-a>indole-1,3(2H,4H)-dione (155794-86-8) + (4'aR*,5'S*)-8,8'-dimethoxy-5,4'a-di<1-(methoxyimino)ethyl>-2,2'-diphenyl-4'a,5'-dihydro-4,5'-bi<1,3,5>triazino<1,2-a>indole-1,3,1',3'(2H,4H,2'H,4'H)-tetraone + (10'S,10'aS)-7'-Methoxy-10,10'a-bis-{1-[(E)-methoxyimino]-ethyl}-3,3'-diphenyl-10',10'a-dihydro-1'H-[1,10']bi[[1,3,5]triazino[1,2-a]indolyl]-2,4,2',4'-tetraone

Guidance literature:

In benzene; Irradiation;

DOI:10.1246/bcsj.69.3533

Downstream raw materials:

8-methoxy-5-<1-(methoxyimino)ethyl>-2-phenyl<1,3,5>triazino<1,2-a>indole-1,3(2H,4H)-dione

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