6,6-bis(3-(triisopropylsilyloxy)benzyl)cyclohex-1-enyl trifluoromethanesulfonate

Base Information

Chemical Name:6,6-bis(3-(triisopropylsilyloxy)benzyl)cyclohex-1-enyl trifluoromethanesulfonate
CAS No.:1204322-38-2
Molecular Formula:C₃₉H₆₁F₃O₅SSi₂
Molecular Weight:755.143
Hs Code.:

Synonyms:6,6-bis(3-(triisopropylsilyloxy)benzyl)cyclohex-1-enyl trifluoromethanesulfonate

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Chemical Property of 6,6-bis(3-(triisopropylsilyloxy)benzyl)cyclohex-1-enyl trifluoromethanesulfonate

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Technology Process of 6,6-bis(3-(triisopropylsilyloxy)benzyl)cyclohex-1-enyl trifluoromethanesulfonate

There total 1 articles about 6,6-bis(3-(triisopropylsilyloxy)benzyl)cyclohex-1-enyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1204322-52-0
C₃₈H₆₂O₃Si₂

: 145100-50-1
1,1,1-trifluoro-N-(pyridin-2-yl)-N-((trifluoromethyl)sulfonyl)methane sulfonamide

: 1204322-38-2
6,6-bis(3-(triisopropylsilyloxy)benzyl)cyclohex-1-enyl trifluoromethanesulfonate

Guidance literature:: C₃₈H₆₂O₃Si₂; With potassium hexamethylsilazane; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

1,1,1-trifluoro-N-(pyridin-2-yl)-N-((trifluoromethyl)sulfonyl)methane sulfonamide; In tetrahydrofuran; at -78 - 23 ℃; Inert atmosphere;
DOI:10.1002/anie.200905060

Reference yield: 70.0%

: 1204322-38-2
6,6-bis(3-(triisopropylsilyloxy)benzyl)cyclohex-1-enyl trifluoromethanesulfonate

: 1204322-25-7
(R)-triisopropyl(3-((7-(triisopropylsilyloxy)-2,3,9,9a-tetrahydro-1H-fluoren-9a-yl)methyl)phenoxy)silane

Guidance literature:: With (3aR,8aR)-N,N-dibutyl-4,4,8,8-tetrakis(4-tert-butylphenyl)-2,2-dimethyltetrahydro-[1,3]dioxolo[4,5-e][1,3,2]dioxaphosphepin-6-amine; palladium diacetate; sodium hydrogencarbonate; In N,N-dimethyl acetamide; at 23 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/anie.200905060