2-acetoxymethyl-3-hydroxy-1,1,3-trimethyl-6-phenylselenoxycyclohexane

Base Information

Chemical Name:2-acetoxymethyl-3-hydroxy-1,1,3-trimethyl-6-phenylselenoxycyclohexane
CAS No.:73527-21-6
Molecular Formula:C₁₈H₂₆O₄Se
Molecular Weight:385.362
Hs Code.:

Synonyms:2-acetoxymethyl-3-hydroxy-1,1,3-trimethyl-6-phenylselenoxycyclohexane

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Chemical Property of 2-acetoxymethyl-3-hydroxy-1,1,3-trimethyl-6-phenylselenoxycyclohexane

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Technology Process of 2-acetoxymethyl-3-hydroxy-1,1,3-trimethyl-6-phenylselenoxycyclohexane

There total 5 articles about 2-acetoxymethyl-3-hydroxy-1,1,3-trimethyl-6-phenylselenoxycyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.2%

: 73527-20-5,85545-22-8,122273-92-1
2-acetoxymethyl-3-hydroxy-1,1,3-trimethyl-6-phenylselenylcyclohexane

: 73527-21-6
2-acetoxymethyl-3-hydroxy-1,1,3-trimethyl-6-phenylselenoxycyclohexane

Guidance literature:: With dihydrogen peroxide; In methanol; at 0 ℃; for 0.166667h;
DOI:10.1248/cpb.29.105

Reference yield:

: 105-87-3,8022-83-1
3,7-dimethyl-2E,6-octadien-1-yl acetate

: 73527-21-6
2-acetoxymethyl-3-hydroxy-1,1,3-trimethyl-6-phenylselenoxycyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: 25 percent / NaOAc / acetic acid / 0.25 h / Ambient temperature

2: 65 percent / trifluoroacetic acid / CH₂Cl₂ / 0.25 h / 0 °C

3: 46.2 percent / 30percent H₂O₂ / methanol / 0.17 h / 0 °C

With dihydrogen peroxide; sodium acetate; trifluoroacetic acid; In methanol; dichloromethane; acetic acid;
DOI:10.1248/cpb.29.105

Reference yield:

: 37715-31-4
(E)-5-(3,3-dimethyloxiran-2-yl)-3-methylpent-2-enyl acetate

: 73527-21-6
2-acetoxymethyl-3-hydroxy-1,1,3-trimethyl-6-phenylselenoxycyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaBH₄ / 1.) ethanol, r.t., 15 min; 2.) ethanol, r.t., 1.5 h

2: 65 percent / trifluoroacetic acid / CH₂Cl₂ / 0.25 h / 0 °C

3: 46.2 percent / 30percent H₂O₂ / methanol / 0.17 h / 0 °C

With sodium tetrahydroborate; dihydrogen peroxide; trifluoroacetic acid; In methanol; dichloromethane;
DOI:10.1248/cpb.29.105