4-(dibutylamino)-3,5-dinitrobenzenesulfonyl chloride

Base Information

Chemical Name:4-(dibutylamino)-3,5-dinitrobenzenesulfonyl chloride
CAS No.:908843-99-2
Molecular Formula:C₁₄H₂₀ClN₃O₆S
Molecular Weight:393.848
Hs Code.:

Synonyms:4-(dibutylamino)-3,5-dinitrobenzenesulfonyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(dibutylamino)-3,5-dinitrobenzenesulfonyl chloride

Chemical Property:

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Technology Process of 4-(dibutylamino)-3,5-dinitrobenzenesulfonyl chloride

There total 7 articles about 4-(dibutylamino)-3,5-dinitrobenzenesulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: potassium 3,5-dinitro-N⁴,N⁴-di-n-butylsulfonate

: 908843-99-2
4-(dibutylamino)-3,5-dinitrobenzenesulfonyl chloride

Guidance literature:: With phosphorus pentachloride; In dichloromethane; for 2h;
DOI:10.1021/jm0304461 DOI:10.1016/j.bmc.2006.04.017

Reference yield:

: 38185-06-7
potassium 4-chloro-3,5-dinitrobenzene sulfonate

: 908843-99-2
4-(dibutylamino)-3,5-dinitrobenzenesulfonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / methanol / Heating

2: PCl₅ / CH₂Cl₂ / 2 h

With phosphorus pentachloride; triethylamine; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2006.04.017

Reference yield:

: 111-92-2
dibutylamine

: 908843-99-2
4-(dibutylamino)-3,5-dinitrobenzenesulfonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / methanol / 3 h / Heating

2: PCl₅ / CH₂Cl₂ / 2 h

With phosphorus pentachloride; In methanol; dichloromethane;
DOI:10.1021/jm0304461