N-benzyloxycarbonyl-glutamic acid diamide

Base Information

Chemical Name:N-benzyloxycarbonyl-glutamic acid diamide
CAS No.:92043-67-9
Molecular Formula:C₁₃H₁₇N₃O₄
Molecular Weight:279.296
Hs Code.:

<i>N</i>-benzyloxycarbonyl-glutamic acid diamide

Synonyms:N-benzyloxycarbonyl-glutamic acid diamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyloxycarbonyl-glutamic acid diamide

Chemical Property:

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Technology Process of N-benzyloxycarbonyl-glutamic acid diamide

There total 14 articles about N-benzyloxycarbonyl-glutamic acid diamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 32668-18-1
Z-Gln-Ser-OMe

: 76491-40-2,92043-67-9,2650-66-0
Cbz-L-Gln-NH₂

Guidance literature:: With ruthenium trichloride; sodium periodate; In tetrachloromethane; acetonitrile; for 1.5h; Ambient temperature; pH 3;
DOI:10.1021/ja00094a008

Reference yield: 74.0%

: 2650-64-8
Cbz-L-Gln

: 76491-40-2,92043-67-9,2650-66-0
Cbz-L-Gln-NH₂

Guidance literature:: Cbz-L-Gln; With chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; at 0 ℃; for 0.5h;

With ammonium chloride; In tetrahydrofuran; water; at 0 ℃; for 0.5h;
DOI:10.1016/j.tetasy.2017.10.015

Reference yield:

: C₁₃H₁₆N₂O₅*H₃N

: 76491-40-2,92043-67-9,2650-66-0
Cbz-L-Gln-NH₂

Guidance literature:: With Bacillus licheniformis serine endoprotease; ammonia; In 1,4-dioxane; N,N-dimethyl-formamide; tert-butyl alcohol; at 50 ℃; for 16h; Molecular sieve; Enzymatic reaction;
DOI:10.1016/j.tetlet.2012.05.039