dimethyl (1-acetamido-2-phenylvinyl)phosphonate

Base Information

Chemical Name:dimethyl (1-acetamido-2-phenylvinyl)phosphonate
CAS No.:436157-42-5
Molecular Formula:C₁₂H₁₆NO₄P
Molecular Weight:269.237
Hs Code.:

Synonyms:dimethyl (1-acetamido-2-phenylvinyl)phosphonate

Suppliers and Price of dimethyl (1-acetamido-2-phenylvinyl)phosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of dimethyl (1-acetamido-2-phenylvinyl)phosphonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of dimethyl (1-acetamido-2-phenylvinyl)phosphonate

There total 1 articles about dimethyl (1-acetamido-2-phenylvinyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 18793-44-7,18793-45-8,1722-84-5
N-β-styrylacetamid

: 868-85-9
Dimethyl phosphite

: 436157-42-5
dimethyl (1-acetamido-2-phenylvinyl)phosphonate

Guidance literature:: With manganese(III) acetylacetonate; In toluene; for 24h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.orglett.9b03174

Reference yield: 99.0%

: 436157-42-5
dimethyl (1-acetamido-2-phenylvinyl)phosphonate

: dimethyl (1-acetamido-2-phenylethyl)phosphonate

Guidance literature:: With bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; (R_c,R_a)-PEAPhos; hydrogen; In 2,2,2-trifluoroethanol; at 25 ℃; for 24h; under 45004.5 Torr; enantioselective reaction; Autoclave; Glovebox;
DOI:10.1021/acs.orglett.9b03174

Reference yield:

: 436157-42-5
dimethyl (1-acetamido-2-phenylvinyl)phosphonate

: C₁₂H₁₈NO₄P

Guidance literature:: With C₃₆H₃₂N₃O₃P; bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen; In dichloromethane; at 20 ℃; for 3h; under 3800.26 Torr; optical yield given as %ee; enantioselective reaction; Autoclave;
DOI:10.1002/anie.201104912