ethyl 3-benzoylaminocarbonyloxy-3-(4-chlorophenyl)-2-methylenepropanoate

Base Information

Chemical Name:ethyl 3-benzoylaminocarbonyloxy-3-(4-chlorophenyl)-2-methylenepropanoate
CAS No.:741716-59-6
Molecular Formula:C₂₀H₁₈ClNO₅
Molecular Weight:387.82
Hs Code.:

Synonyms:ethyl 3-benzoylaminocarbonyloxy-3-(4-chlorophenyl)-2-methylenepropanoate

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Chemical Property of ethyl 3-benzoylaminocarbonyloxy-3-(4-chlorophenyl)-2-methylenepropanoate

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Technology Process of ethyl 3-benzoylaminocarbonyloxy-3-(4-chlorophenyl)-2-methylenepropanoate

There total 3 articles about ethyl 3-benzoylaminocarbonyloxy-3-(4-chlorophenyl)-2-methylenepropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 147849-98-7
ethyl 2-((4-chlorophenyl)(hydroxy)methyl)acrylate

: 4461-33-0
benzoyl isocyanate

: 741716-59-6
ethyl 3-benzoylaminocarbonyloxy-3-(4-chlorophenyl)-2-methylenepropanoate

Guidance literature:: In dichloromethane; at 20 ℃; for 3h;
DOI:10.1021/ol049146j

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 741716-59-6
ethyl 3-benzoylaminocarbonyloxy-3-(4-chlorophenyl)-2-methylenepropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / DABCO / 360 h / 20 °C

2: 100 percent / CH₂Cl₂ / 3 h / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; In dichloromethane; 1: Baylis-Hillman reaction;
DOI:10.1021/ol049146j

Reference yield:

: 140-88-5,9003-32-1
ethyl acrylate

: 741716-59-6
ethyl 3-benzoylaminocarbonyloxy-3-(4-chlorophenyl)-2-methylenepropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / DABCO / 360 h / 20 °C

2: 100 percent / CH₂Cl₂ / 3 h / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; In dichloromethane; 1: Baylis-Hillman reaction;
DOI:10.1021/ol049146j