ethyl (2S,4S,6S)-4,6-di(1H-indol-3-yl)-1-phenylpiperidine-2-carboxylate

Base Information

Chemical Name:ethyl (2S,4S,6S)-4,6-di(1H-indol-3-yl)-1-phenylpiperidine-2-carboxylate
CAS No.:1608150-18-0
Molecular Formula:C₃₀H₂₉N₃O₂
Molecular Weight:463.579
Hs Code.:

Synonyms:ethyl (2S,4S,6S)-4,6-di(1H-indol-3-yl)-1-phenylpiperidine-2-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl (2S,4S,6S)-4,6-di(1H-indol-3-yl)-1-phenylpiperidine-2-carboxylate

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Technology Process of ethyl (2S,4S,6S)-4,6-di(1H-indol-3-yl)-1-phenylpiperidine-2-carboxylate

There total 6 articles about ethyl (2S,4S,6S)-4,6-di(1H-indol-3-yl)-1-phenylpiperidine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 53654-36-7
3-vinyl-1H-indole

: 121642-09-9,84484-31-1
ethyl 2-(phenylimino)acetate

: 1608150-18-0
ethyl (2S,4S,6S)-4,6-di(1H-indol-3-yl)-1-phenylpiperidine-2-carboxylate

: ethyl (2R,4R,6R)-4,6-di(1H-indol-3-yl)-1-phenylpiperidine-2-carboxylate

Guidance literature:: With (R)‐3,3′‐bis(9‐phenanthryl)‐1,1′‐binaphthalene‐2,2′‐diyl hydrogen phosphate; In acetonitrile; at 20 ℃; for 1.5h; Reagent/catalyst; Solvent; Temperature; enantioselective reaction; Catalytic behavior; Inert atmosphere;
DOI:10.1039/c4ob00234b

Reference yield: 40.0%

: 53654-36-7
3-vinyl-1H-indole

: 121642-09-9,84484-31-1
ethyl 2-(phenylimino)acetate

: 1608150-18-0
ethyl (2S,4S,6S)-4,6-di(1H-indol-3-yl)-1-phenylpiperidine-2-carboxylate

Guidance literature:: With (R)‐3,3′‐bis(9‐phenanthryl)‐1,1′‐binaphthalene‐2,2′‐diyl hydrogen phosphate; In dichloromethane; at 25 ℃; for 1h; enantioselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201701502

Reference yield: 30.0%

: 924-44-7
glyoxylic acid ethyl ester

: 53654-36-7
3-vinyl-1H-indole

: 62-53-3
aniline

: 1608150-18-0
ethyl (2S,4S,6S)-4,6-di(1H-indol-3-yl)-1-phenylpiperidine-2-carboxylate

Guidance literature:: With (R)‐3,3′‐bis(9‐phenanthryl)‐1,1′‐binaphthalene‐2,2′‐diyl hydrogen phosphate; magnesium sulfate; In dichloromethane; at 20 ℃; for 1h; Reagent/catalyst; Solvent; Temperature; enantioselective reaction; Inert atmosphere;
DOI:10.1039/c4ob00234b