o-(cyanomethyl)benzylcyanamide

Base Information

Chemical Name:o-(cyanomethyl)benzylcyanamide
CAS No.:145083-89-2
Molecular Formula:C₁₀H₉N₃
Molecular Weight:171.202
Hs Code.:

Synonyms:o-(cyanomethyl)benzylcyanamide

Suppliers and Price of o-(cyanomethyl)benzylcyanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of o-(cyanomethyl)benzylcyanamide

Chemical Property:

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Technology Process of o-(cyanomethyl)benzylcyanamide

There total 4 articles about o-(cyanomethyl)benzylcyanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 139702-90-2
5-(o-cyanomethyl)benzylamino-1,2,3,4-thiatriazole

: 145083-89-2
o-(cyanomethyl)benzylcyanamide

Guidance literature:: In benzene; at 70 ℃; for 3h;
DOI:10.1016/S0040-4020(01)90364-3

Reference yield:

: 73217-11-5
(2-bromomethylphenyl)acetonitrile

: 145083-89-2
o-(cyanomethyl)benzylcyanamide

Guidance literature:: Multi-step reaction with 4 steps

1: sodium iodide / dimethylformamide / 90 °C

2: 50 percent aq. hydrazine / ethanol / Ambient temperature

3: aq. sodium nitrite, 10 percent hydrochloric acid / Ambient temperature

4: 90 percent / benzene / 3 h / 70 °C

With hydrogenchloride; hydrazine hydrate; sodium iodide; sodium nitrite; In ethanol; N,N-dimethyl-formamide; benzene;
DOI:10.1016/S0040-4020(01)90364-3

Reference yield:

: 401571-90-2
(2-Isothiocyanatomethyl-phenyl)-acetonitrile

: 145083-89-2
o-(cyanomethyl)benzylcyanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent aq. hydrazine / ethanol / Ambient temperature

2: aq. sodium nitrite, 10 percent hydrochloric acid / Ambient temperature

3: 90 percent / benzene / 3 h / 70 °C

With hydrogenchloride; hydrazine hydrate; sodium nitrite; In ethanol; benzene;
DOI:10.1016/S0040-4020(01)90364-3