2-tert-butoxycarbonylamino-3-(2S)-tert-butoxycarbonylamino-3-((2S)phenyl propionylsulfanyl)propionic acid methyl ester

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Chemical Name:2-tert-butoxycarbonylamino-3-(2S)-tert-butoxycarbonylamino-3-((2S)phenyl propionylsulfanyl)propionic acid methyl ester
CAS No.:1333435-26-9
Molecular Formula:C₂₃H₃₄N₂O₇S
Molecular Weight:482.598
Hs Code.:

Synonyms:2-tert-butoxycarbonylamino-3-(2S)-tert-butoxycarbonylamino-3-((2S)phenyl propionylsulfanyl)propionic acid methyl ester

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Chemical Property of 2-tert-butoxycarbonylamino-3-(2S)-tert-butoxycarbonylamino-3-((2S)phenyl propionylsulfanyl)propionic acid methyl ester

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Technology Process of 2-tert-butoxycarbonylamino-3-(2S)-tert-butoxycarbonylamino-3-((2S)phenyl propionylsulfanyl)propionic acid methyl ester

There total 2 articles about 2-tert-butoxycarbonylamino-3-(2S)-tert-butoxycarbonylamino-3-((2S)phenyl propionylsulfanyl)propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1333435-21-4
2-((S)-tert-butoxycarbonylamino)-3-phenylpropionic acid 4-chlorophenyl ester

: 172749-96-1
(S)-methyl 2-((tert-butoxycarbonyl)amino)-3-mercaptopropanoate

: 1333435-26-9
2-tert-butoxycarbonylamino-3-(2S)-tert-butoxycarbonylamino-3-((2S)phenyl propionylsulfanyl)propionic acid methyl ester

Guidance literature:: With [Bu₄N][Fe(CO)₃(NO)]; In 1,4-dioxane; at 20 - 80 ℃; for 24h; optical yield given as %de; Molecular sieve; Inert atmosphere;
DOI:10.1002/chem.201101073

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 1333435-26-9
2-tert-butoxycarbonylamino-3-(2S)-tert-butoxycarbonylamino-3-((2S)phenyl propionylsulfanyl)propionic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C

2: [Bu₄N][Fe(CO)₃(NO)] / 1,4-dioxane / 24 h / 20 - 80 °C / Molecular sieve; Inert atmosphere

With dmap; dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane;
DOI:10.1002/chem.201101073