2-((S)-tert-butoxycarbonylamino)-3-phenylpropionic acid 4-chlorophenyl ester

Base Information

Chemical Name:2-((S)-tert-butoxycarbonylamino)-3-phenylpropionic acid 4-chlorophenyl ester
CAS No.:1333435-21-4
Molecular Formula:C₂₀H₂₂ClNO₄
Molecular Weight:375.852
Hs Code.:

Synonyms:2-((S)-tert-butoxycarbonylamino)-3-phenylpropionic acid 4-chlorophenyl ester

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Chemical Property of 2-((S)-tert-butoxycarbonylamino)-3-phenylpropionic acid 4-chlorophenyl ester

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Technology Process of 2-((S)-tert-butoxycarbonylamino)-3-phenylpropionic acid 4-chlorophenyl ester

There total 1 articles about 2-((S)-tert-butoxycarbonylamino)-3-phenylpropionic acid 4-chlorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 106-48-9,82344-39-6
4-chloro-phenol

: 1333435-21-4
2-((S)-tert-butoxycarbonylamino)-3-phenylpropionic acid 4-chlorophenyl ester

Guidance literature:: With sodium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; ethyl cyanoglyoxylate-2-oxime; In water; acetonitrile; at 20 ℃; for 2h;
DOI:10.1021/ol3022337 DOI:10.1021/ol3022337

Reference yield: 96.0%

: 1333435-21-4
2-((S)-tert-butoxycarbonylamino)-3-phenylpropionic acid 4-chlorophenyl ester

: 100-53-8
phenylmethanethiol

: 95364-14-0
(S)-2-tert-butoxycarbonylamino-3-phenylthiopropionic acid S-benzyl ester

Guidance literature:: With [Bu₄N][Fe(CO)₃(NO)]; In 1,4-dioxane; at 20 - 80 ℃; for 16h; optical yield given as %ee; Molecular sieve; Inert atmosphere;
DOI:10.1002/chem.201101073

Reference yield: 96.0%

: 1333435-21-4
2-((S)-tert-butoxycarbonylamino)-3-phenylpropionic acid 4-chlorophenyl ester

: 172749-96-1
(S)-methyl 2-((tert-butoxycarbonyl)amino)-3-mercaptopropanoate

: 1333435-26-9
2-tert-butoxycarbonylamino-3-(2S)-tert-butoxycarbonylamino-3-((2S)phenyl propionylsulfanyl)propionic acid methyl ester

Guidance literature:: With [Bu₄N][Fe(CO)₃(NO)]; In 1,4-dioxane; at 20 - 80 ℃; for 24h; optical yield given as %de; Molecular sieve; Inert atmosphere;
DOI:10.1002/chem.201101073