1,4-diiodo-2,5-bis(11-(tert-butoxycarbonyl)-3,6,9-trioxaundecyloxy)benzene

Base Information

Chemical Name:1,4-diiodo-2,5-bis(11-(tert-butoxycarbonyl)-3,6,9-trioxaundecyloxy)benzene
CAS No.:1274917-84-8
Molecular Formula:C₃₂H₅₂I₂O₁₂
Molecular Weight:882.567
Hs Code.:

Synonyms:1,4-diiodo-2,5-bis(11-(tert-butoxycarbonyl)-3,6,9-trioxaundecyloxy)benzene

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Chemical Property of 1,4-diiodo-2,5-bis(11-(tert-butoxycarbonyl)-3,6,9-trioxaundecyloxy)benzene

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Technology Process of 1,4-diiodo-2,5-bis(11-(tert-butoxycarbonyl)-3,6,9-trioxaundecyloxy)benzene

There total 6 articles about 1,4-diiodo-2,5-bis(11-(tert-butoxycarbonyl)-3,6,9-trioxaundecyloxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 217817-01-1
tert-butyl 3-[2-[2-[2-(4-methylphenyl)sulfonyloxyethoxy]ethoxy]ethoxy]propanoate

: 13064-64-7
2,5-diiodo-1,4-hydroquinone

: 1274917-84-8
1,4-diiodo-2,5-bis(11-(tert-butoxycarbonyl)-3,6,9-trioxaundecyloxy)benzene

Guidance literature:: With 18-crown-6 ether; potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 100 ℃; for 48h; Inert atmosphere;
DOI:10.1139/V10-156

Reference yield:

: 186020-66-6,892154-71-1
3-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethoxy}-propionic acid tert-butyl ester

: 1274917-84-8
1,4-diiodo-2,5-bis(11-(tert-butoxycarbonyl)-3,6,9-trioxaundecyloxy)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 4 - 20 °C

2: potassium carbonate; potassium iodide / butanone / 38 h / Reflux

With potassium carbonate; triethylamine; potassium iodide; In dichloromethane; butanone;
DOI:10.1002/adfm.201102027

Reference yield:

: 150-78-7
1,4-dimethoxybezene

: 1274917-84-8
1,4-diiodo-2,5-bis(11-(tert-butoxycarbonyl)-3,6,9-trioxaundecyloxy)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid; iodine; acetic acid / water

2: boron tribromide / dichloromethane

3: potassium carbonate; potassium iodide / butanone / 38 h / Reflux

With sulfuric acid; iodine; boron tribromide; potassium carbonate; acetic acid; potassium iodide; In dichloromethane; water; butanone;
DOI:10.1002/adfm.201102027