C₄₄H₂₈OS

Base Information

Chemical Name:C₄₄H₂₈OS
CAS No.:1402419-90-2
Molecular Formula:C₄₄H₂₈OS
Molecular Weight:604.772
Hs Code.:

Synonyms:C₄₄H₂₈OS

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₄H₂₈OS

Chemical Property:

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Technology Process of C₄₄H₂₈OS

There total 3 articles about C₄₄H₂₈OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1402419-89-9
C₃₂H₁₈OS

: 82214-69-5
2-biphenylmagnesium bromide

: 1402419-90-2
C₄₄H₂₈OS

Guidance literature:: C₃₂H₁₈OS; 2-biphenylmagnesium bromide; In tetrahydrofuran; at 20 ℃; for 5h; Inert atmosphere; Cooling with ice;

With water; In tetrahydrofuran; Cooling with ice;

Reference yield:

: 132-65-0
dibenzothiophene

: 1402419-90-2
C₄₄H₂₈OS

Guidance literature:: Multi-step reaction with 5 steps

1.1: aluminum (III) chloride / dichloromethane / 3 h / 20 °C / Cooling with ice

1.2: 1 h / Cooling with ice

2.1: polyphosphoric acid / chloroform / 5 h / 80 °C / Inert atmosphere; Cooling with ice

3.1: tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Cooling with ice

3.2: Cooling with ice

4.1: hydrogenchloride; acetic acid / water / 5 h / 100 °C / Inert atmosphere

5.1: tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Cooling with ice

5.2: Cooling with ice

With hydrogenchloride; aluminum (III) chloride; acetic acid; In tetrahydrofuran; dichloromethane; chloroform; water;

Reference yield:

: 31123-60-1
2-(o-carboxybenzoyl)dibenzothiophene

: 1402419-90-2
C₄₄H₂₈OS

Guidance literature:: Multi-step reaction with 4 steps

1.1: polyphosphoric acid / chloroform / 5 h / 80 °C / Inert atmosphere; Cooling with ice

2.1: tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Cooling with ice

2.2: Cooling with ice

3.1: hydrogenchloride; acetic acid / water / 5 h / 100 °C / Inert atmosphere

4.1: tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Cooling with ice

4.2: Cooling with ice

With hydrogenchloride; acetic acid; In tetrahydrofuran; chloroform; water;