3,4-difluorophenyl tert-butyl(2,3-difluoro-6-vinyloxyphenyl)phosphinate

Base Information

Chemical Name:3,4-difluorophenyl tert-butyl(2,3-difluoro-6-vinyloxyphenyl)phosphinate
CAS No.:1224895-39-9
Molecular Formula:C₁₈H₁₇F₄O₃P
Molecular Weight:388.299
Hs Code.:

Synonyms:3,4-difluorophenyl tert-butyl(2,3-difluoro-6-vinyloxyphenyl)phosphinate

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Chemical Property of 3,4-difluorophenyl tert-butyl(2,3-difluoro-6-vinyloxyphenyl)phosphinate

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Technology Process of 3,4-difluorophenyl tert-butyl(2,3-difluoro-6-vinyloxyphenyl)phosphinate

There total 3 articles about 3,4-difluorophenyl tert-butyl(2,3-difluoro-6-vinyloxyphenyl)phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.9%

: 1224895-84-4
3,4-difluorophenyl tert-butyl(2,3-difluoro-6-hydroxyphenyl)phosphinate

: 1112-56-7
tetravinyltin (IV)

: 1224895-39-9
3,4-difluorophenyl tert-butyl(2,3-difluoro-6-vinyloxyphenyl)phosphinate

Guidance literature:: With oxygen; copper diacetate; In acetonitrile; at 20 ℃; for 20h;
DOI:10.1002/adsc.200900304

Reference yield:

: 1224895-74-2
tert-butylphosphonic acid di(3,4-difluorophenyl) ester

: 1224895-39-9
3,4-difluorophenyl tert-butyl(2,3-difluoro-6-vinyloxyphenyl)phosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium / tetrahydrofuran / -78 - 20 °C

2: oxygen; copper diacetate / acetonitrile / 20 h / 20 °C

With n-butyllithium; oxygen; copper diacetate; In tetrahydrofuran; acetonitrile;
DOI:10.1002/adsc.200900304

Reference yield:

: 2713-33-9
3,4-difluorophenol

: 1224895-39-9
3,4-difluorophenyl tert-butyl(2,3-difluoro-6-vinyloxyphenyl)phosphinate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran / 1 h / 0 °C

2: n-butyllithium / tetrahydrofuran / -78 - 20 °C

3: oxygen; copper diacetate / acetonitrile / 20 h / 20 °C

With n-butyllithium; oxygen; copper diacetate; sodium hydride; In tetrahydrofuran; acetonitrile;
DOI:10.1002/adsc.200900304