6-methyl-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2(1H),4(3H),7(8H)-pteridinetrione

Base Information

Chemical Name:6-methyl-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2(1H),4(3H),7(8H)-pteridinetrione
CAS No.:73978-94-6
Molecular Formula:C₃₃H₂₆N₄O₁₀
Molecular Weight:638.59
Hs Code.:

Synonyms:6-methyl-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2(1H),4(3H),7(8H)-pteridinetrione

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Chemical Property of 6-methyl-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2(1H),4(3H),7(8H)-pteridinetrione

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Technology Process of 6-methyl-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2(1H),4(3H),7(8H)-pteridinetrione

There total 7 articles about 6-methyl-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2(1H),4(3H),7(8H)-pteridinetrione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 73978-97-9
2,4-Bis(benzyloxy)-6-methyl-7-oxo-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-7,8-dihydropteridin

: 73978-94-6
6-methyl-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2(1H),4(3H),7(8H)-pteridinetrione

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; Ambient temperature;

Reference yield: 58.0%

: 701285-12-3
4-benzyloxy-6-methyl-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2(1H),7(8H)-pteridinedione

: 73978-94-6
6-methyl-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2(1H),4(3H),7(8H)-pteridinetrione

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 48h;
DOI:10.1081/NCN-120027817

Reference yield:

: 6974-32-9
1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose

: 73978-94-6
6-methyl-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2(1H),4(3H),7(8H)-pteridinetrione

Guidance literature:: Multi-step reaction with 5 steps

1.1: (NH₄)2SO₄; hexamethyldisilazane / 6 h / Heating

1.2: 45 percent / BF₃-etherate / CH₂Cl₂ / 24 h / 20 °C

2.1: silver carbonate / benzene / 2 h / 80 °C

2.2: 14 percent / benzene / 48 h / 60 - 70 °C

3.1: 92 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 12 h

4.1: 28 percent / aq. NaOH / tetrahydrofuran / 6 h

5.1: 58 percent / H₂ / Pd/C / ethyl acetate / 48 h

With ammonium sulfate; sodium hydroxide; hydrogen; 3-chloro-benzenecarboperoxoic acid; 1,1,1,3,3,3-hexamethyl-disilazane; silver carbonate; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; ethyl acetate; benzene;
DOI:10.1081/NCN-120027817