6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione

Base Information

Chemical Name:6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione
CAS No.:701285-00-9
Molecular Formula:C₃₄H₂₈N₄O₉S
Molecular Weight:668.684
Hs Code.:

Synonyms:6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione

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Chemical Property of 6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione

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Technology Process of 6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione

There total 1 articles about 6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 6974-32-9
1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose

: 138612-37-0
6-methyl-2-methylthio-4(3H),7(8H)-pteridinedione

: 701285-00-9
6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione

Guidance literature:: 6-methyl-2-methylthio-4(3H),7(8H)-pteridinedione; With ammonium sulfate; 1,1,1,3,3,3-hexamethyl-disilazane; for 6h; Heating;

1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose; With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1081/NCN-120027817

Reference yield: 61.0%

: 701285-00-9
6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione

: 100-39-0
benzyl bromide

: 701285-03-2
4-benzyloxy-6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione

: 701285-04-3
3-benzyl-6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione

Guidance literature:: 6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione; With silver carbonate; In benzene; at 80 ℃; for 2h;

benzyl bromide; In benzene; at 60 - 70 ℃; for 48h;
DOI:10.1081/NCN-120027817

Reference yield:

: 701285-00-9
6-methyl-2-methylthio-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4(3H),7(8H)-pteridinedione

: 73978-94-6
6-methyl-8-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2(1H),4(3H),7(8H)-pteridinetrione

Guidance literature:: Multi-step reaction with 4 steps

1.1: silver carbonate / benzene / 2 h / 80 °C

1.2: 14 percent / benzene / 48 h / 60 - 70 °C

2.1: 92 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 12 h

3.1: 28 percent / aq. NaOH / tetrahydrofuran / 6 h

4.1: 58 percent / H₂ / Pd/C / ethyl acetate / 48 h

With sodium hydroxide; hydrogen; 3-chloro-benzenecarboperoxoic acid; silver carbonate; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; ethyl acetate; benzene;
DOI:10.1081/NCN-120027817