benzyloxy(triethoxy)silane

Base Information

• Chemical Name: benzyloxy(triethoxy)silane
• CAS No.: 122205-34-9
• Molecular Formula: C₁₃H₂₂O₄Si
• Molecular Weight: 270.401
• Mol file: 122205-34-9.mol

Synonyms:benzyloxy(triethoxy)silane

Chemical Property of benzyloxy(triethoxy)silane

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of benzyloxy(triethoxy)silane

There total 17 articles about benzyloxy(triethoxy)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

Triethoxysilane (998-30-1) + benzoic acid ethyl ester (93-89-0,99341-95-4) → benzyloxy(triethoxy)silane (122205-34-9)

Guidance literature:

With hydroxyapatite; In n-heptane; at 90 ℃; for 20h;

DOI:10.1246/bcsj.66.2638

Reference yield: 93.0%

triethoxysilyl formate + benzyl alcohol (100-51-6,185532-71-2) → benzyloxy(triethoxy)silane (122205-34-9)

Guidance literature:

With [Ru(κ¹-OAc)(κ²-OAc)(κ³-1,1,1-tris(diphenylphosphinomethyl)ethane)]; In acetonitrile; at 70 ℃; for 18h; Inert atmosphere; Schlenk technique; Sealed tube;

Reference yield: 72.0%

Triethoxysilane (998-30-1) + benzaldehyde (100-52-7) → benzyloxy(triethoxy)silane (122205-34-9)

Guidance literature:

hydroxyapatite; In n-heptane; at 90 ℃; for 2h;

DOI:10.1016/S0040-4039(00)92296-2

upstream raw materials:

Triethoxysilane

benzoic acid ethyl ester

benzaldehyde

[Zn(OCH₂C₆H₅)((dimethylamino)ethanol)]2

Downstream raw materials:

benzyl alcohol