2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)-1,1-ethanol

Base Information

• Chemical Name: 2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)-1,1-ethanol
• CAS No.: 148729-73-1
• Molecular Formula: C₂₆H₂₈N₄O₅S
• Molecular Weight: 508.598

Synonyms:2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)-1,1-ethanol

Chemical Property of 2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)-1,1-ethanol

Chemical Property:

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Technology Process of 2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)-1,1-ethanol

There total 19 articles about 2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)-1,1-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)ketone (125335-95-7) → 2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)-1,1-ethanol (148729-73-1)

Guidance literature:

With ammonium chloride; methyllithium; In diethyl ether; ethanol;

Reference yield: 91.0%

methyllithium (917-54-4) + 2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)ketone (125335-95-7) → 2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)-1,1-ethanol (148729-73-1)

Guidance literature:

In tetrahydrofuran; diethyl ether; at -20 ℃; for 0.166667h;

DOI:10.1016/S0040-4020(01)80387-2

Reference yield: 45.0%

→ 2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)-1,1-ethanol (148729-73-1)

Guidance literature:

upstream raw materials:

methyllithium

2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)-4-(3-diethylaminocarbonyl-2-methoxypyridyl)ketone

methylmagnesium chloride

1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine

Downstream raw materials:

1-<2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)>-1,3-dihydro-1,3-dimethyl-3-hydroxy-4-methoxyfuro<3,4-c>pyridine

1-<2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)>-1,3-dihydro-3,4-dimethoxy-1-methylfuro<3,4-c>pyridine

1-<2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)>-1,3-dihydro-3-hydroxy-4-methoxy-1-methylfuro<3,4-c>pyridine

1-<2-(1-Benzenesulfonyl-1H-pyrrolo<3,2-c>pyridine)>-1,3-dihydro-4-methoxy-1-methyl-3-oxofuro<3,4-c>pyridine

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