N-(5'-O-acetyl-2',3'-O-isopropylidene-α-D-ribofuranosyl)-4,5-dimethyl-2-nitrobenzenamine

Base Information

Chemical Name:N-(5'-O-acetyl-2',3'-O-isopropylidene-α-D-ribofuranosyl)-4,5-dimethyl-2-nitrobenzenamine
CAS No.:312715-35-8
Molecular Formula:C₁₈H₂₄N₂O₇
Molecular Weight:380.398
Hs Code.:

Synonyms:N-(5'-O-acetyl-2',3'-O-isopropylidene-α-D-ribofuranosyl)-4,5-dimethyl-2-nitrobenzenamine

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Chemical Property of N-(5'-O-acetyl-2',3'-O-isopropylidene-α-D-ribofuranosyl)-4,5-dimethyl-2-nitrobenzenamine

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Technology Process of N-(5'-O-acetyl-2',3'-O-isopropylidene-α-D-ribofuranosyl)-4,5-dimethyl-2-nitrobenzenamine

There total 3 articles about N-(5'-O-acetyl-2',3'-O-isopropylidene-α-D-ribofuranosyl)-4,5-dimethyl-2-nitrobenzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 108-24-7
acetic anhydride

: 312715-34-7
N-(2',3'-O-isopropylidene-α-D-ribofuranosyl)-4,5-dimethyl-2-nitrobenzenamine

: 312715-35-8
N-(5'-O-acetyl-2',3'-O-isopropylidene-α-D-ribofuranosyl)-4,5-dimethyl-2-nitrobenzenamine

Guidance literature:: In pyridine; at 50 ℃; for 8h;
DOI:10.1002/1522-2675(20000906)83:9<2452::AID-HLCA2452>3.0.CO;2-6

Reference yield:

: 67814-68-0,70266-87-4,76249-50-8,76249-51-9,93451-15-1,4099-88-1
2,3-O-isopropylidene-D-ribofuranose

: 312715-35-8
N-(5'-O-acetyl-2',3'-O-isopropylidene-α-D-ribofuranosyl)-4,5-dimethyl-2-nitrobenzenamine

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / NH₄Cl / ethanol / 2.5 h / Heating

2: 98 percent / pyridine / 8 h / 50 °C

With ammonium chloride; In pyridine; ethanol; 1: Condensation / 2: Acetylation;
DOI:10.1002/1522-2675(20000906)83:9<2452::AID-HLCA2452>3.0.CO;2-6

Reference yield:

: 6972-71-0
4,5-dimethyl-2-nitrobenzenamine

: 312715-35-8
N-(5'-O-acetyl-2',3'-O-isopropylidene-α-D-ribofuranosyl)-4,5-dimethyl-2-nitrobenzenamine

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / NH₄Cl / ethanol / 2.5 h / Heating

2: 98 percent / pyridine / 8 h / 50 °C

With ammonium chloride; In pyridine; ethanol; 1: Condensation / 2: Acetylation;
DOI:10.1002/1522-2675(20000906)83:9<2452::AID-HLCA2452>3.0.CO;2-6