N-(2',3'-O-isopropylidene-α-D-ribofuranosyl)-4,5-dimethyl-2-nitrobenzenamine

Base Information

Chemical Name:N-(2',3'-O-isopropylidene-α-D-ribofuranosyl)-4,5-dimethyl-2-nitrobenzenamine
CAS No.:312715-34-7
Molecular Formula:C₁₆H₂₂N₂O₆
Molecular Weight:338.36
Hs Code.:

Synonyms:N-(2',3'-O-isopropylidene-α-D-ribofuranosyl)-4,5-dimethyl-2-nitrobenzenamine

Suppliers and Price of N-(2',3'-O-isopropylidene-α-D-ribofuranosyl)-4,5-dimethyl-2-nitrobenzenamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(2',3'-O-isopropylidene-α-D-ribofuranosyl)-4,5-dimethyl-2-nitrobenzenamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(2',3'-O-isopropylidene-α-D-ribofuranosyl)-4,5-dimethyl-2-nitrobenzenamine

There total 1 articles about N-(2',3'-O-isopropylidene-α-D-ribofuranosyl)-4,5-dimethyl-2-nitrobenzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 67814-68-0,70266-87-4,76249-50-8,76249-51-9,93451-15-1,4099-88-1
2,3-O-isopropylidene-D-ribofuranose

: 6972-71-0
4,5-dimethyl-2-nitrobenzenamine

: 312715-34-7
N-(2',3'-O-isopropylidene-α-D-ribofuranosyl)-4,5-dimethyl-2-nitrobenzenamine

: N-(2',3'-O-isopropylidene-β-D-ribofuranosyl)-4,5-dimethyl-2-nitrobenzenamine

Guidance literature:: With ammonium chloride; In ethanol; for 2.5h; Heating;
DOI:10.1002/1522-2675(20000906)83:9<2452::AID-HLCA2452>3.0.CO;2-6

Reference yield: 98.0%

: 108-24-7
acetic anhydride

: 312715-34-7
N-(2',3'-O-isopropylidene-α-D-ribofuranosyl)-4,5-dimethyl-2-nitrobenzenamine

: 312715-35-8
N-(5'-O-acetyl-2',3'-O-isopropylidene-α-D-ribofuranosyl)-4,5-dimethyl-2-nitrobenzenamine

Guidance literature:: In pyridine; at 50 ℃; for 8h;
DOI:10.1002/1522-2675(20000906)83:9<2452::AID-HLCA2452>3.0.CO;2-6

Reference yield:

: 312715-34-7
N-(2',3'-O-isopropylidene-α-D-ribofuranosyl)-4,5-dimethyl-2-nitrobenzenamine

: Acetic acid (3aR,4R,6S,6aR)-6-(2-amino-4,5-dimethyl-phenylamino)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / pyridine / 8 h / 50 °C

2: H₂; Et₃N / PO₂ / ethyl acetate / 1 h / 1500.12 Torr

With hydrogen; triethylamine; PO₂; In pyridine; ethyl acetate; 1: Acetylation / 2: Reduction;
DOI:10.1002/1522-2675(20000906)83:9<2452::AID-HLCA2452>3.0.CO;2-6