bis(2-methoxyphenyl)(phenyl)((3-(trifluoromethyl)phenyl)ethynyl)phosphonium bromide

Base Information

Chemical Name:bis(2-methoxyphenyl)(phenyl)((3-(trifluoromethyl)phenyl)ethynyl)phosphonium bromide
CAS No.:1620057-24-0
Molecular Formula:Br*C₂₉H₂₃F₃O₂P
Molecular Weight:571.373
Hs Code.:

Synonyms:bis(2-methoxyphenyl)(phenyl)((3-(trifluoromethyl)phenyl)ethynyl)phosphonium bromide

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Chemical Property of bis(2-methoxyphenyl)(phenyl)((3-(trifluoromethyl)phenyl)ethynyl)phosphonium bromide

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Technology Process of bis(2-methoxyphenyl)(phenyl)((3-(trifluoromethyl)phenyl)ethynyl)phosphonium bromide

There total 3 articles about bis(2-methoxyphenyl)(phenyl)((3-(trifluoromethyl)phenyl)ethynyl)phosphonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 33675-48-8
1-(bromoethynyl)-3-(trifluoromethyl)benzene

: 36802-41-2
bis-(2-methoxy-phenyl)-phenyl-phosphane

: 1620057-24-0
bis(2-methoxyphenyl)(phenyl)((3-(trifluoromethyl)phenyl)ethynyl)phosphonium bromide

Guidance literature:: In toluene; at 45 ℃; for 72h;
DOI:10.1039/c4cc03415e

Reference yield:

: 644-97-3
Dichlorophenylphosphine

: 1620057-24-0
bis(2-methoxyphenyl)(phenyl)((3-(trifluoromethyl)phenyl)ethynyl)phosphonium bromide

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium / tetrahydrofuran / 1 h / 60 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: toluene / 72 h / 45 °C

With magnesium; In tetrahydrofuran; toluene;
DOI:10.1039/c4cc03415e

Reference yield:

: 578-57-4
2-bromoanisole

: 1620057-24-0
bis(2-methoxyphenyl)(phenyl)((3-(trifluoromethyl)phenyl)ethynyl)phosphonium bromide

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium / tetrahydrofuran / 1 h / 60 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: toluene / 72 h / 45 °C

With magnesium; In tetrahydrofuran; toluene;
DOI:10.1039/c4cc03415e