Technology Process of C21H31N5O7SSi
There total 7 articles about C21H31N5O7SSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
at 20 ℃;
for 20h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ammonium hydroxide / tetrahydrofuran / 16 h / 20 °C
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 h / 20 °C
With
ammonium hydroxide; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: trifluoroacetic acid / 0.5 h / 20 °C
1.2: 5 - 20 °C
2.1: trichlorophosphate; N,N-dimethyl-aniline / 2 h / 0 - 100 °C
3.1: triethylamine; ammonia / tetrahydrofuran; isopropyl alcohol / 5 h / 20 °C
4.1: triethylamine / tetrahydrofuran / 6 h / 20 °C
5.1: potassium carbonate; sodium iodide / acetone / 16 h / 20 °C
6.1: ammonium hydroxide / tetrahydrofuran / 16 h / 20 °C
7.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 h / 20 °C
With
ammonium hydroxide; ammonia; potassium carbonate; N,N-dimethyl-aniline; triethylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; sodium iodide; trichlorophosphate;
In
tetrahydrofuran; dichloromethane; isopropyl alcohol; acetone;