1,3-bis-(bromomethyl)-5-[((4,6-dimethylpyridin-2-yl)amino)methyl]-2,4,6-triethylbenzene

Base Information

• Chemical Name: 1,3-bis-(bromomethyl)-5-[((4,6-dimethylpyridin-2-yl)amino)methyl]-2,4,6-triethylbenzene
• CAS No.: 1030362-76-5
• Molecular Formula: C₂₂H₃₀Br₂N₂
• Molecular Weight: 482.302

Synonyms:1,3-bis-(bromomethyl)-5-[((4,6-dimethylpyridin-2-yl)amino)methyl]-2,4,6-triethylbenzene

Chemical Property of 1,3-bis-(bromomethyl)-5-[((4,6-dimethylpyridin-2-yl)amino)methyl]-2,4,6-triethylbenzene

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Technology Process of 1,3-bis-(bromomethyl)-5-[((4,6-dimethylpyridin-2-yl)amino)methyl]-2,4,6-triethylbenzene

There total 2 articles about 1,3-bis-(bromomethyl)-5-[((4,6-dimethylpyridin-2-yl)amino)methyl]-2,4,6-triethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

2-Amino-4,6-dimethylpyridine (5407-87-4) + 1,3,5-tris(bromomethyl)-2,4,6-triethylbenzene (181058-08-2) → 1-(bromomethyl)-3,5-bis[((4,6-dimethylpyridin-2-yl)amino)-methyl]-2,4,6-triethylbenzene + 1,3-bis-(bromomethyl)-5-[((4,6-dimethylpyridin-2-yl)amino)methyl]-2,4,6-triethylbenzene (1030362-76-5) + 1,3,5-tris-[(4,6-dimethyl-pyridin-2-yl)-aminomethyl]-2,4,6-triethylbenzene (797818-01-0)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; acetonitrile; at 20 ℃; for 48h;

DOI:10.1002/chem.200701269

Reference yield: 20.0%

2-Amino-4,6-dimethylpyridine (5407-87-4) + 1,3,5-tris(bromomethyl)-2,4,6-triethylbenzene (181058-08-2) → 1,3-bis-(bromomethyl)-5-[((4,6-dimethylpyridin-2-yl)amino)methyl]-2,4,6-triethylbenzene (1030362-76-5)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; acetonitrile; at 20 ℃; for 72h;

DOI:10.1021/jo100982x

Reference yield: 71.0%

1,3-bis-(bromomethyl)-5-[((4,6-dimethylpyridin-2-yl)amino)methyl]-2,4,6-triethylbenzene (1030362-76-5) + isobutylamine (78-81-9) → 1,3-bis[(isobutylamino)methyl]-5-[(4,6-dimethylpyridin-2-yl)-aminomethyl]-2,4,6-triethylbenzene (1246878-48-7)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; acetonitrile; at 20 ℃; for 24h;

DOI:10.1021/jo100982x

upstream raw materials:

2-Amino-4,6-dimethylpyridine

1,3,5-tris(bromomethyl)-2,4,6-triethylbenzene

Downstream raw materials:

1,3-bis[(isobutylamino)methyl]-5-[(4,6-dimethylpyridin-2-yl)-aminomethyl]-2,4,6-triethylbenzene

1,3-bis(aminomethyl)-5-[(4,6-dimethylpyridin-2-yl)aminomethyl]-2,4,6-triethylbenzene

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