[2-(Benzhydrylidene-amino)-2-methoxycarbonyl-ethyl]-trimethyl-ammonium; iodide

Base Information

• Chemical Name: [2-(Benzhydrylidene-amino)-2-methoxycarbonyl-ethyl]-trimethyl-ammonium; iodide
• CAS No.: 118553-18-7
• Molecular Formula: C₂₀H₂₅N₂O₂*I
• Molecular Weight: 452.335

Synonyms:[2-(Benzhydrylidene-amino)-2-methoxycarbonyl-ethyl]-trimethyl-ammonium; iodide

Chemical Property of [2-(Benzhydrylidene-amino)-2-methoxycarbonyl-ethyl]-trimethyl-ammonium; iodide

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of [2-(Benzhydrylidene-amino)-2-methoxycarbonyl-ethyl]-trimethyl-ammonium; iodide

There total 2 articles about [2-(Benzhydrylidene-amino)-2-methoxycarbonyl-ethyl]-trimethyl-ammonium; iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-(Benzhydrylidene-amino)-3-dimethylamino-propionic acid methyl ester (118553-15-4) + methyl iodide (74-88-4) → [2-(Benzhydrylidene-amino)-2-methoxycarbonyl-ethyl]-trimethyl-ammonium; iodide (118553-18-7)

Guidance literature:

In ethanol; for 10h; Ambient temperature;

DOI:10.1055/s-1988-27621

Reference yield:

methyl N-(diphenylmethylene)glycinate (81167-39-7) → [2-(Benzhydrylidene-amino)-2-methoxycarbonyl-ethyl]-trimethyl-ammonium; iodide (118553-18-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 63 percent / CH₂Cl₂ / 12 h / Ambient temperature

2: 90 percent / ethanol / 10 h / Ambient temperature

In ethanol; dichloromethane;

DOI:10.1055/s-1988-27621

Reference yield: 93.0%

[2-(Benzhydrylidene-amino)-2-methoxycarbonyl-ethyl]-trimethyl-ammonium; iodide (118553-18-7) → Methyl N-(diphenylmethylene)-α,β-didehydroalaninate (118553-21-2)

Guidance literature:

With potassium carbonate; In methanol; for 16h; Ambient temperature;

DOI:10.1055/s-1988-27621

upstream raw materials:

2-(Benzhydrylidene-amino)-3-dimethylamino-propionic acid methyl ester

methyl iodide

methyl N-(diphenylmethylene)glycinate

Downstream raw materials:

Methyl N-(diphenylmethylene)-α,β-didehydroalaninate

Methyl N-(diphenylmethylene)-D,L-tryptophanates

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