C₃₉H₅₃N₃O₇

Base Information

Chemical Name:C₃₉H₅₃N₃O₇
CAS No.:1056681-45-8
Molecular Formula:C₃₉H₅₃N₃O₇
Molecular Weight:675.866
Hs Code.:

C<sub>39</sub>H<sub>53</sub>N<sub>3</sub>O<sub>7</sub>

Synonyms:C₃₉H₅₃N₃O₇

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Chemical Property of C₃₉H₅₃N₃O₇

Chemical Property:

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Technology Process of C₃₉H₅₃N₃O₇

There total 18 articles about C₃₉H₅₃N₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1056674-78-2
acetic acid (1S,3S)-3-((S)-1-benzylcarbamoyl-2-methylpropylcarbamoyl)-1-((S)-1-tert-butoxycarbonylamino-2-hydroxy-ethyl)-4-methylpentyl ester

: 1056674-82-8
1-(naphthalen-1-yl)ethyl 2,2,2-trichloroacetimidate

: 1056681-45-8
C₃₉H₅₃N₃O₇

Guidance literature:: boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 17h;

Reference yield:

: 1056674-54-4
(3S,5S)-5-[(1R)-2-(benzyloxy)-1-hydroxyethyl]-3-isopropyldihydrofuran-2(3H)-one

: 1056681-45-8
C₃₉H₅₃N₃O₇

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine / dichloromethane / 0.25 - 0.5 h / 0 - 20 °C

2: sodium azide / N,N-dimethyl-formamide / 1 h / 60 °C

3: 2-hydroxypyridin; N-ethyl-N,N-diisopropylamine / 72 h / 70 °C

4: hydrogen / palladium, 5% on calcium carbonate, poisoned with lead / ethyl acetate

5: dmap / dichloromethane / 0.25 h / 20 °C

6: hydrogen / palladium 10% on activated carbon / methanol

7: boron trifluoride diethyl etherate / dichloromethane / 17 h / 20 °C

With pyridine; 2-hydroxypyridin; dmap; sodium azide; hydrogen; N-ethyl-N,N-diisopropylamine; palladium, 5% on calcium carbonate, poisoned with lead; palladium 10% on activated carbon; boron trifluoride diethyl etherate; In methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 13734-41-3
t-Boc-L-valine

: 1056681-45-8
C₃₉H₅₃N₃O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 0.08 h / 0 °C

1.2: 0.33 h

2.1: trifluoroacetic acid / 1 h / 20 °C

3.1: 2-hydroxypyridin; N-ethyl-N,N-diisopropylamine / 72 h / 70 °C

4.1: hydrogen / palladium, 5% on calcium carbonate, poisoned with lead / ethyl acetate

5.1: dmap / dichloromethane / 0.25 h / 20 °C

6.1: hydrogen / palladium 10% on activated carbon / methanol

7.1: boron trifluoride diethyl etherate / dichloromethane / 17 h / 20 °C

With 2-hydroxypyridin; dmap; hydrogen; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; palladium, 5% on calcium carbonate, poisoned with lead; palladium 10% on activated carbon; boron trifluoride diethyl etherate; In methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;