Benzenepropanoic acid, alpha,alpha-dimethyl-beta-[(1-methylsilacyclobut-1-yl)oxy]-, methyl ester

Base Information

Chemical Name:Benzenepropanoic acid, alpha,alpha-dimethyl-beta-[(1-methylsilacyclobut-1-yl)oxy]-, methyl ester
CAS No.:146645-08-1
Molecular Formula:C₁₆H₂₄O₃Si
Molecular Weight:292.45
Hs Code.:
DSSTox Substance ID:DTXSID601127976
Nikkaji Number:J598.048H

Synonyms:DTXSID601127976;146645-08-1

Suppliers and Price of Benzenepropanoic acid, alpha,alpha-dimethyl-beta-[(1-methylsilacyclobut-1-yl)oxy]-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenepropanoic acid, alpha,alpha-dimethyl-beta-[(1-methylsilacyclobut-1-yl)oxy]-, methyl ester

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:292.14947116
Heavy Atom Count:20
Complexity:344

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C(C1=CC=CC=C1)O[Si]2(CCC2)C)C(=O)OC

Technology Process of Benzenepropanoic acid, alpha,alpha-dimethyl-beta-[(1-methylsilacyclobut-1-yl)oxy]-, methyl ester

There total 2 articles about Benzenepropanoic acid, alpha,alpha-dimethyl-beta-[(1-methylsilacyclobut-1-yl)oxy]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 100-52-7
benzaldehyde

: 143399-14-8
1-<(1-methoxy-2-methyl-1-propenyl)oxy>-1-methylsilacyclobutane

: 146645-08-1
methyl 2,2-dimethyl-3-<1-(1-methylsilacyclobutoxy)>-3-phenylpropanoate

Guidance literature:: In benzene; at 27 ℃; for 4h;
DOI:10.1021/ja00046a054

Reference yield:

: 547-63-7,133320-07-7,67505-84-4
Methyl isobutyrate

: 146645-08-1
methyl 2,2-dimethyl-3-<1-(1-methylsilacyclobutoxy)>-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) LDA

2: 100 percent / benzene / 4 h / 27 °C

With lithium diisopropyl amide; In benzene;
DOI:10.1021/ja00046a054