(2R)-2-[benzyl{(2-((diphenylphosphanyl)oxy)ethyl)}amino]butyldiphenylphosphinite

Base Information

Chemical Name:(2R)-2-[benzyl{(2-((diphenylphosphanyl)oxy)ethyl)}amino]butyldiphenylphosphinite
CAS No.:1305343-44-5
Molecular Formula:C₃₇H₃₉NO₂P₂
Molecular Weight:591.67
Hs Code.:

Synonyms:(2R)-2-[benzyl{(2-((diphenylphosphanyl)oxy)ethyl)}amino]butyldiphenylphosphinite

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Chemical Property of (2R)-2-[benzyl{(2-((diphenylphosphanyl)oxy)ethyl)}amino]butyldiphenylphosphinite

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Technology Process of (2R)-2-[benzyl{(2-((diphenylphosphanyl)oxy)ethyl)}amino]butyldiphenylphosphinite

There total 2 articles about (2R)-2-[benzyl{(2-((diphenylphosphanyl)oxy)ethyl)}amino]butyldiphenylphosphinite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 352655-19-7
(R)-(-)-N-benzyl-4-hydroxymethyl-3-azahexan-1-ol

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 1305343-44-5
(2R)-2-[benzyl{(2-((diphenylphosphanyl)oxy)ethyl)}amino]butyldiphenylphosphinite

Guidance literature:: With triethylamine; In toluene; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.jorganchem.2010.12.027

Reference yield:

: 6257-49-4,51977-20-9
(2R)-2-(benzylamino)butan-1-ol

: 1305343-44-5
(2R)-2-[benzyl{(2-((diphenylphosphanyl)oxy)ethyl)}amino]butyldiphenylphosphinite

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / -20 °C / Inert atmosphere

2: triethylamine / toluene / 0 - 20 °C / Inert atmosphere

With triethylamine; In methanol; toluene;
DOI:10.1016/j.jorganchem.2010.12.027

Reference yield: 86.0%

: 52462-29-0
[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

: 1305343-44-5
(2R)-2-[benzyl((2-((diphenylphosphanyl)oxy)ethyl))amino]butyldiphenylphosphinite

: μ-(2R)-2-[benzyl((2-((diphenylphosphanyl)oxy)ethyl))amino]butyldiphenylphosphinito-bis[dichloro(η6-p-isopropyltoluene)ruthenium(II)]

Guidance literature:: In toluene; Schlenk techniques used under Ar, (Ru(η6-p-cumene)(μ-Cl)Cl)2 (0.44 mmol) and 1 (0.44 mmol) dissolved in toluene, stirred for 6 h at room temp.; concentrated under vac., petroleum ether added, filtered, dried; elem. anal.;
DOI:10.1016/j.jorganchem.2010.12.027