4-cyanobenzoate phenethyl ester

Base Information

• Chemical Name: 4-cyanobenzoate phenethyl ester
• CAS No.: 131786-46-4
• Molecular Formula: C₁₆H₁₃NO₂
• Molecular Weight: 251.285

Synonyms:4-cyanobenzoate phenethyl ester

Chemical Property of 4-cyanobenzoate phenethyl ester

Chemical Property:

Purity/Quality:

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Technology Process of 4-cyanobenzoate phenethyl ester

There total 9 articles about 4-cyanobenzoate phenethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2-phenylethanol (60-12-8) + 4-cyanobenzaldehyde (105-07-7) → 4-cyanobenzoate phenethyl ester (131786-46-4)

Guidance literature:

With sodium cyanide; copper(l) iodide; In neat (no solvent); at 120 ℃; for 20h;

DOI:10.1002/aoc.3766

Reference yield: 81.0%

2-phenylethanol (60-12-8) + 4-iodobenzonitrile (3058-39-7) + molybdenum hexacarbonyl (13939-06-5,199620-15-0) → 4-cyanobenzoate phenethyl ester (131786-46-4)

Guidance literature:

With tributyl-amine; In N,N-dimethyl-formamide; at 80 ℃; for 2.7h;

DOI:10.1039/c6ra18679c

Reference yield: 75.0%

2-phenylethanol (60-12-8) + 4-iodobenzonitrile (3058-39-7) + chromium(0) hexacarbonyl (199620-14-9,13007-92-6) → 4-cyanobenzoate phenethyl ester (131786-46-4)

Guidance literature:

With triethylamine; nickel dichloride; In N,N-dimethyl-formamide; at 100 ℃; for 1.3h;

DOI:10.1039/c5nj00655d

upstream raw materials:

pyridine-2-carboxylic acid phenethyl ester

4-cyanobenzaldehyde

2-phenylethanol

4-cyanophenyl methyl ketone

Downstream raw materials:

2-<4-<(phenethyloxy)carbonyl>phenyl>-4-hydroxy-5-methylthiazole

styrene

1-methoxy-2-phenylethane

4-cyanobenzoic Acid

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