Technology Process of C15H21NO5S
There total 5 articles about C15H21NO5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
at 0 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 20 °C
2: sodium hydrogencarbonate / toluene / 20 °C
3: sodium tetrahydroborate / tetrahydrofuran / 1 h / 0 - 20 °C
4: triethylamine / dichloromethane / 0.5 h / 0 °C
With
sodium tetrahydroborate; hydrogen; sodium hydrogencarbonate; triethylamine;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; dichloromethane; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium tert-butylate; Methyltriphenylphosphonium bromide / diethyl ether / 3.42 h / 5 - 35 °C
2: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 20 °C
3: sodium hydrogencarbonate / toluene / 20 °C
4: sodium tetrahydroborate / tetrahydrofuran / 1 h / 0 - 20 °C
5: triethylamine / dichloromethane / 0.5 h / 0 °C
With
sodium tetrahydroborate; potassium tert-butylate; hydrogen; Methyltriphenylphosphonium bromide; sodium hydrogencarbonate; triethylamine;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene;