(S)-1-(2,2-diphenylacetyl)-4-(3-phenylpropyl)piperazine-2-carboxylic acid

Base Information

Chemical Name:(S)-1-(2,2-diphenylacetyl)-4-(3-phenylpropyl)piperazine-2-carboxylic acid
CAS No.:1448678-92-9
Molecular Formula:C₂₈H₃₀N₂O₃
Molecular Weight:442.558
Hs Code.:

Synonyms:(S)-1-(2,2-diphenylacetyl)-4-(3-phenylpropyl)piperazine-2-carboxylic acid

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Chemical Property of (S)-1-(2,2-diphenylacetyl)-4-(3-phenylpropyl)piperazine-2-carboxylic acid

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Technology Process of (S)-1-(2,2-diphenylacetyl)-4-(3-phenylpropyl)piperazine-2-carboxylic acid

There total 6 articles about (S)-1-(2,2-diphenylacetyl)-4-(3-phenylpropyl)piperazine-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 1448678-91-8
(S)-4-cinnamyl-1-(2,2-diphenylacetyl)piperazine-2-carboxylic acid

: 1448678-92-9
(S)-1-(2,2-diphenylacetyl)-4-(3-phenylpropyl)piperazine-2-carboxylic acid

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethyl acetate; at 20 ℃; under 760.051 Torr;

Reference yield:

: 1448679-18-2
C₂₀H₂₈N₂O₄

: 1448678-92-9
(S)-1-(2,2-diphenylacetyl)-4-(3-phenylpropyl)piperazine-2-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: trifluoroacetic acid / dichloromethane / 20 °C

2: triethylamine / dichloromethane / 0.17 h / 0 - 20 °C

3: lithium hydroxide monohydrate / tetrahydrofuran; water / 20 °C

4: palladium 10% on activated carbon; hydrogen / ethyl acetate / 20 °C / 760.05 Torr

With lithium hydroxide monohydrate; palladium 10% on activated carbon; hydrogen; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; ethyl acetate;

Reference yield:

: 796096-64-5
(S)-piperazine-1,2-dicarboxylic acid 1-tert-butyl ester 2-methyl ester

: 1448678-92-9
(S)-1-(2,2-diphenylacetyl)-4-(3-phenylpropyl)piperazine-2-carboxylic acid

Guidance literature:: Multi-step reaction with 5 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 5 h / 0 - 20 °C

2: trifluoroacetic acid / dichloromethane / 20 °C

3: triethylamine / dichloromethane / 0.17 h / 0 - 20 °C

4: lithium hydroxide monohydrate / tetrahydrofuran; water / 20 °C

5: palladium 10% on activated carbon; hydrogen / ethyl acetate / 20 °C / 760.05 Torr

With lithium hydroxide monohydrate; palladium 10% on activated carbon; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;