N¹-[1-(2-hydroxy-1-naphthyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline]-N²-p-chlorophenylthiourea

Base Information

• Chemical Name: N¹-[1-(2-hydroxy-1-naphthyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline]-N²-p-chlorophenylthiourea
• CAS No.: 1047998-26-4
• Molecular Formula: C₂₈H₂₅ClN₂O₃S
• Molecular Weight: 505.037

Synonyms:N¹-[1-(2-hydroxy-1-naphthyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline]-N²-p-chlorophenylthiourea

Chemical Property of N¹-[1-(2-hydroxy-1-naphthyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline]-N²-p-chlorophenylthiourea

Chemical Property:

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Technology Process of N¹-[1-(2-hydroxy-1-naphthyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline]-N²-p-chlorophenylthiourea

There total 1 articles about N¹-[1-(2-hydroxy-1-naphthyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline]-N²-p-chlorophenylthiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-(6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)-2-naphthol (897035-07-3) + 4-Chlorophenyl isothiocyanate (2131-55-7) → N1-[1-(2-hydroxy-1-naphthyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline]-N2-p-chlorophenylthiourea (1047998-26-4)

Guidance literature:

In toluene; at 20 ℃; for 24h;

DOI:10.1016/j.tet.2008.05.025

Reference yield:

N1-[1-(2-hydroxy-1-naphthyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline]-N2-p-chlorophenylthiourea (1047998-26-4) + methyl iodide (74-88-4) → C29H27ClN2O3S

Guidance literature:

In methanol; for 20h;

DOI:10.1016/j.tet.2008.05.025

upstream raw materials:

1-(6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)-2-naphthol

4-Chlorophenyl isothiocyanate

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