(Z)-1-(1-benzofuran-2-yl)-1-t-butyldimethylsilyloxy-2-(4-methoxyphenyl)ethene

Base Information

Chemical Name:(Z)-1-(1-benzofuran-2-yl)-1-t-butyldimethylsilyloxy-2-(4-methoxyphenyl)ethene
CAS No.:1384131-23-0
Molecular Formula:C₂₃H₂₈O₃Si
Molecular Weight:380.559
Hs Code.:

Synonyms:(Z)-1-(1-benzofuran-2-yl)-1-t-butyldimethylsilyloxy-2-(4-methoxyphenyl)ethene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-1-(1-benzofuran-2-yl)-1-t-butyldimethylsilyloxy-2-(4-methoxyphenyl)ethene

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Technology Process of (Z)-1-(1-benzofuran-2-yl)-1-t-butyldimethylsilyloxy-2-(4-methoxyphenyl)ethene

There total 3 articles about (Z)-1-(1-benzofuran-2-yl)-1-t-butyldimethylsilyloxy-2-(4-methoxyphenyl)ethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1183881-43-7
1-(benzofuran-2-yl)-2-(4-methoxyphenyl)ethan-1-one

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1384131-23-0
(Z)-1-(1-benzofuran-2-yl)-1-t-butyldimethylsilyloxy-2-(4-methoxyphenyl)ethene

Guidance literature:: With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 - 20 ℃; for 4h;
DOI:10.1055/s-0031-1290528

Reference yield:

: 267884-96-8
N-methoxy-2-(4-methoxyphenyl)-N-methylethanamide

: 1384131-23-0
(Z)-1-(1-benzofuran-2-yl)-1-t-butyldimethylsilyloxy-2-(4-methoxyphenyl)ethene

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C

1.2: 1.5 h / 20 °C

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 4 h / -78 - 20 °C

With n-butyllithium; sodium hexamethyldisilazane; In tetrahydrofuran; hexane;
DOI:10.1055/s-0031-1290528

Reference yield:

: 271-89-6
1-benzofurane

: 1384131-23-0
(Z)-1-(1-benzofuran-2-yl)-1-t-butyldimethylsilyloxy-2-(4-methoxyphenyl)ethene

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C

1.2: 1.5 h / 20 °C

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 4 h / -78 - 20 °C

With n-butyllithium; sodium hexamethyldisilazane; In tetrahydrofuran; hexane;
DOI:10.1055/s-0031-1290528