2-dimethoxymethyl-6-fluorobenzoic acid

Base Information

Chemical Name:2-dimethoxymethyl-6-fluorobenzoic acid
CAS No.:717816-83-6
Molecular Formula:C₁₀H₁₁FO₄
Molecular Weight:214.193
Hs Code.:

Synonyms:2-dimethoxymethyl-6-fluorobenzoic acid

Suppliers and Price of 2-dimethoxymethyl-6-fluorobenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-dimethoxymethyl-6-fluorobenzoic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-dimethoxymethyl-6-fluorobenzoic acid

There total 1 articles about 2-dimethoxymethyl-6-fluorobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124-38-9,18923-20-1
carbon dioxide

: 717816-83-6
2-dimethoxymethyl-6-fluorobenzoic acid

Guidance literature:: α,α-dimethoxy-m-fluorotoluene; With sec.-butyllithium; In tetrahydrofuran; cyclohexane; at -78 ℃; for 3h;

carbon dioxide; In tetrahydrofuran; cyclohexane; at -78 - 20 ℃; for 1h;

With hydrogenchloride; In tetrahydrofuran; cyclohexane; water;

Reference yield:

: 717816-83-6
2-dimethoxymethyl-6-fluorobenzoic acid

: 2-chloro-6-(8-fluoro-1-oxo-1H-phthalazin-2-yl)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine; acetic acid / isopropyl alcohol / 2 h / 100 °C / Reflux; Inert atmosphere

2: caesium carbonate / N,N-dimethyl acetamide / 24 h / 55 °C

With caesium carbonate; acetic acid; hydrazine; In N,N-dimethyl acetamide; isopropyl alcohol;

Reference yield:

: 717816-83-6
2-dimethoxymethyl-6-fluorobenzoic acid

: 2-(3-chloro-2-hydroxymethylphenyl)-8-fluoro-2H-phthalazin-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine; acetic acid / isopropyl alcohol / 2 h / 100 °C / Reflux; Inert atmosphere

2: caesium carbonate / N,N-dimethyl acetamide / 24 h / 55 °C

3: sodium tetrahydroborate; isopropyl alcohol / N,N-dimethyl acetamide / 20 °C

With sodium tetrahydroborate; caesium carbonate; acetic acid; isopropyl alcohol; hydrazine; In N,N-dimethyl acetamide; isopropyl alcohol;