(+/-)-tert-butyl (1-((allyl(benzyl)amino)carbonyl)but-3-en-1-yl)carbamate

Base Information

Chemical Name:(+/-)-tert-butyl (1-((allyl(benzyl)amino)carbonyl)but-3-en-1-yl)carbamate
CAS No.:918306-87-3
Molecular Formula:C₂₀H₂₈N₂O₃
Molecular Weight:344.454
Hs Code.:

Synonyms:(+/-)-tert-butyl (1-((allyl(benzyl)amino)carbonyl)but-3-en-1-yl)carbamate

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Chemical Property of (+/-)-tert-butyl (1-((allyl(benzyl)amino)carbonyl)but-3-en-1-yl)carbamate

Chemical Property:

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Technology Process of (+/-)-tert-butyl (1-((allyl(benzyl)amino)carbonyl)but-3-en-1-yl)carbamate

There total 1 articles about (+/-)-tert-butyl (1-((allyl(benzyl)amino)carbonyl)but-3-en-1-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 4383-22-6
Allylbenzylamine

: 119479-32-2
2-((tert-butyloxycarbonyl)amino)-4-pentenoic acid

: 918306-87-3
(+/-)-tert-butyl (1-((allyl(benzyl)amino)carbonyl)but-3-en-1-yl)carbamate

Guidance literature:: With 1-methyl-pyrrolidin-2-one; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1016/j.bmc.2006.09.009

Reference yield: 82.0%

: 918306-87-3
(+/-)-tert-butyl (1-((allyl(benzyl)amino)carbonyl)but-3-en-1-yl)carbamate

: 183867-13-2
(+/-)-tert-butyl (1-benzyl-2-oxo-2,3,4,7-tetrahydro-1H-azepin-3-yl)carbamate

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 65 ℃;
DOI:10.1021/ol501529z

Reference yield:

: 918306-87-3
(+/-)-tert-butyl (1-((allyl(benzyl)amino)carbonyl)but-3-en-1-yl)carbamate

: C₁₈H₂₆N₂O₅

Guidance literature:: Multi-step reaction with 2 steps

1.1: 76 percent / (PCy₃)2Cl₂Ru(=CHPh) / CH₂Cl₂ / 24 h / Heating

2.1: potassium osmate; potassium carbonate; potassium ferricyanide / methane sulfonamide / 2-methyl-propan-2-ol; H₂O / 48 h / 0 - 20 °C

2.2: sodium sulfite / 2-methyl-propan-2-ol; H₂O / 20 °C

With potassium osmate(VI); potassium carbonate; potassium hexacyanoferrate(III); Grubbs catalyst first generation; methanesulfonamide; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.bmc.2006.09.009