2,9-dimethyl-4,7-diphenyl-1,10-phenanthroline bis[(2-diphenyl-phosphino)phenyl]ether copper(I) hexafluorophosphate

Base Information

• Chemical Name: 2,9-dimethyl-4,7-diphenyl-1,10-phenanthroline bis[(2-diphenyl-phosphino)phenyl]ether copper(I) hexafluorophosphate
• CAS No.: 1421057-27-3
• Molecular Formula: C₆₂H₄₈CuN₂OP₂*F₆P
• Molecular Weight: 1107.53
• Mol file: 1421057-27-3.mol

Synonyms:2,9-dimethyl-4,7-diphenyl-1,10-phenanthroline bis[(2-diphenyl-phosphino)phenyl]ether copper(I) hexafluorophosphate

Chemical Property of 2,9-dimethyl-4,7-diphenyl-1,10-phenanthroline bis[(2-diphenyl-phosphino)phenyl]ether copper(I) hexafluorophosphate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,9-dimethyl-4,7-diphenyl-1,10-phenanthroline bis[(2-diphenyl-phosphino)phenyl]ether copper(I) hexafluorophosphate

There total 1 articles about 2,9-dimethyl-4,7-diphenyl-1,10-phenanthroline bis[(2-diphenyl-phosphino)phenyl]ether copper(I) hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

tetrakis(actonitrile)copper(I) hexafluorophosphate (64443-05-6) + Bathocuproine (4733-39-5) + bis[2-(diphenylphosphino)phenyl] ether (166330-10-5) → 2,9-dimethyl-4,7-diphenyl-1,10-phenanthroline bis[(2-diphenyl-phosphino)phenyl]ether copper(I) hexafluorophosphate (1421057-27-3)

Guidance literature:

tetrakis(actonitrile)copper(I) hexafluorophosphate; bis[2-(diphenylphosphino)phenyl] ether; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

Bathocuproine; In dichloromethane; for 1h; Inert atmosphere;

DOI:10.1021/acs.orglett.7b01518

Reference yield:

2,9-dimethyl-4,7-diphenyl-1,10-phenanthroline bis[(2-diphenyl-phosphino)phenyl]ether copper(I) hexafluorophosphate (1421057-27-3) → bis(2,9-dimethyl-4,7-diphenyl-1,10-phenanthroline)copper(I) hexafluorophosphate (47895-81-8) + [copper(I)(bis[2-(diphenylphosphino)phenyl]ether)2](hexafluorophosphate)

Guidance literature:

UV-irradiation;

DOI:10.2533/chimia.2018.621

upstream raw materials:

tetrakis(actonitrile)copper(I) hexafluorophosphate

Bathocuproine

bis[2-(diphenylphosphino)phenyl] ether

Downstream raw materials:

bis(2,9-dimethyl-4,7-diphenyl-1,10-phenanthroline)copper(I) hexafluorophosphate