[H₂BIM(tBu)BPh₂]Cl

Base Information

Chemical Name:[H₂BIM(tBu)BPh₂]Cl
CAS No.:1160462-16-7
Molecular Formula:C₂₆H₃₄BN₄*Cl
Molecular Weight:448.847
Hs Code.:

[H<sub>2</sub>BIM(tBu)BPh<sub>2</sub>]Cl

Synonyms:[H₂BIM(tBu)BPh₂]Cl

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Chemical Property of [H₂BIM(tBu)BPh₂]Cl

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Technology Process of [H₂BIM(tBu)BPh₂]Cl

There total 1 articles about [H₂BIM(tBu)BPh₂]Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.5%

: 3677-81-4
diphenylboronchloride

: 45676-04-8
1-tert-butylimidazole

: 1160462-16-7
[H₂BIM(tBu)BPh₂]Cl

Guidance literature:: In toluene; under Ar; to a soln. of N-tert-butylimidazole (49.2 mmol) in abs. toluene at 0°C was added slowly a soln. of Ph2BCl (18.9 mmol) in abs. toluene; stirring at room temp. for 15 min and then at 110°C for 48 h; the suspn. was filtered under Ar; the ppt. was washed with dry toluene and hexane and then dried at 1E-3 mbar; elem. anal.;
DOI:10.1021/om801097f

Reference yield: 95.3%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 1160462-16-7
[H₂BIM(tBu)BPh₂]Cl

: 2785-29-7
benzyl potassium

: [B(phenyl)₂(3-tert-butyl-2-imidazolyl)(3-tert-butylimidazole-2-ylidene)]K*(thf)n

Guidance literature:: In toluene; at 20 ℃; for 2h; Inert atmosphere; Schlenk technique;
DOI:10.1002/ejic.201500154

Reference yield: 75.0%

: ammonium hexafluorophosphate

: 1160462-16-7
[H₂BIM(tBu)BPh₂]Cl

: 1160462-22-5
[H₂BIM(tBu)BPh₂]PF₆

Guidance literature:: In methanol; to a soln. of B-contg. compd. (6.7 mmol) in MeOH was added in several portions well-milled NH4PF6 (20.1 mmol); stirring at room temp. for several hours; the solids were filtered off and washed on the filter with MeOH; the remaining solid was washed with CH2Cl2 and the filtrate was evapd.; recrystn. from CH2Cl2-MeOH; elem. anal.;
DOI:10.1021/om801097f