Cy₅-tetraglycol-NBA-COOH

Base Information

Chemical Name:Cy₅-tetraglycol-NBA-COOH
CAS No.:1448147-63-4
Molecular Formula:C₄₆H₅₇N₃O₁₄S₂
Molecular Weight:940.102
Hs Code.:

Synonyms:Cy₅-tetraglycol-NBA-COOH

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Chemical Property of Cy₅-tetraglycol-NBA-COOH

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Technology Process of Cy₅-tetraglycol-NBA-COOH

There total 9 articles about Cy₅-tetraglycol-NBA-COOH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 146368-08-3
1-(5-carboxypentyl)-2,3,3-trimethyl-3H-indolium-5-sulfonate

: 1448147-61-2
2,3,3-trimethyl-1-(1-(4-nitrophenyl)-2,5,8,11-tetraoxatridecan-13-yl)-3H-indol-1-ium-5-sulfonate

: 58467-94-0
N-((1E,3E)-3-(phenylimino)prop-1-enyl)benzenamine hydrochloride

: 1448147-63-4
2-((1E,3E,5E)-5-(1-(5-carboxypentyl)-3,3-dimethyl-5-sulfoindolin-2-ylidene)penta-1,3-dien-1-yl)-3,3-dimethyl-1-(-(4-nitrophenyl)-2,5,8,11-tetraoxatridecan-13-yl)-3H-indol-1-ium-5-sulfonate

Guidance literature:: 1-(5-carboxypentyl)-2,3,3-trimethyl-3H-indolium-5-sulfonate; N-((1E,3E)-3-(phenylimino)prop-1-enyl)benzenamine hydrochloride; With acetic anhydride; acetic acid; at 120 ℃; for 2h;

2,3,3-trimethyl-1-(1-(4-nitrophenyl)-2,5,8,11-tetraoxatridecan-13-yl)-3H-indol-1-ium-5-sulfonate; With potassium acetate; at 120 ℃; for 3h;

Reference yield:

: 132557-72-3
2,3,3-trimethylindole-5-sulfonic acid

: 1448147-63-4
2-((1E,3E,5E)-5-(1-(5-carboxypentyl)-3,3-dimethyl-5-sulfoindolin-2-ylidene)penta-1,3-dien-1-yl)-3,3-dimethyl-1-(-(4-nitrophenyl)-2,5,8,11-tetraoxatridecan-13-yl)-3H-indol-1-ium-5-sulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / methanol; isopropyl alcohol / 0.25 h / Reflux

2.1: sulfolane / 16 h / 110 °C / Sealed tube

3.1: acetic anhydride; acetic acid / 2 h / 120 °C

3.2: 3 h / 120 °C

With acetic anhydride; acetic acid; potassium hydroxide; In sulfolane; methanol; isopropyl alcohol;

Reference yield:

: 563-80-4
3-methyl-butan-2-one

: 1448147-63-4
2-((1E,3E,5E)-5-(1-(5-carboxypentyl)-3,3-dimethyl-5-sulfoindolin-2-ylidene)penta-1,3-dien-1-yl)-3,3-dimethyl-1-(-(4-nitrophenyl)-2,5,8,11-tetraoxatridecan-13-yl)-3H-indol-1-ium-5-sulfonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / 3 h / Reflux

2.1: potassium hydroxide / methanol; isopropyl alcohol / 0.25 h / Reflux

3.1: sulfolane / 16 h / 110 °C / Sealed tube

4.1: acetic anhydride; acetic acid / 2 h / 120 °C

4.2: 3 h / 120 °C

With acetic anhydride; acetic acid; potassium hydroxide; In sulfolane; methanol; isopropyl alcohol; 1.1: |Fischer Indole Synthesis;