2,3,3-trimethyl-1-(1-(4-nitrophenyl)-2,5,8,11-tetraoxatridecan-13-yl)-3H-indol-1-ium-5-sulfonate

Base Information

Chemical Name:2,3,3-trimethyl-1-(1-(4-nitrophenyl)-2,5,8,11-tetraoxatridecan-13-yl)-3H-indol-1-ium-5-sulfonate
CAS No.:1448147-61-2
Molecular Formula:C₂₆H₃₄N₂O₉S
Molecular Weight:550.63
Hs Code.:

Synonyms:2,3,3-trimethyl-1-(1-(4-nitrophenyl)-2,5,8,11-tetraoxatridecan-13-yl)-3H-indol-1-ium-5-sulfonate

Suppliers and Price of 2,3,3-trimethyl-1-(1-(4-nitrophenyl)-2,5,8,11-tetraoxatridecan-13-yl)-3H-indol-1-ium-5-sulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,3,3-trimethyl-1-(1-(4-nitrophenyl)-2,5,8,11-tetraoxatridecan-13-yl)-3H-indol-1-ium-5-sulfonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,3,3-trimethyl-1-(1-(4-nitrophenyl)-2,5,8,11-tetraoxatridecan-13-yl)-3H-indol-1-ium-5-sulfonate

There total 7 articles about 2,3,3-trimethyl-1-(1-(4-nitrophenyl)-2,5,8,11-tetraoxatridecan-13-yl)-3H-indol-1-ium-5-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: potassium 2,3,3-trimethylindole-5-sulfonate

: 1448147-59-8
1-bromo-1-(4-nitrophenyl)-2,5,8,11-tetraoxatridecane

: 1448147-61-2
2,3,3-trimethyl-1-(1-(4-nitrophenyl)-2,5,8,11-tetraoxatridecan-13-yl)-3H-indol-1-ium-5-sulfonate

Guidance literature:: In sulfolane; at 110 ℃; for 16h; Sealed tube;

Reference yield:

: 563-80-4
3-methyl-butan-2-one

: 1448147-61-2
2,3,3-trimethyl-1-(1-(4-nitrophenyl)-2,5,8,11-tetraoxatridecan-13-yl)-3H-indol-1-ium-5-sulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / 3 h / Reflux

2: potassium hydroxide / methanol; isopropyl alcohol / 0.25 h / Reflux

3: sulfolane / 16 h / 110 °C / Sealed tube

With acetic acid; potassium hydroxide; In sulfolane; methanol; isopropyl alcohol; 1: |Fischer Indole Synthesis;

Reference yield:

: 112-60-7
Tetraethylene glycol

: 1448147-61-2
2,3,3-trimethyl-1-(1-(4-nitrophenyl)-2,5,8,11-tetraoxatridecan-13-yl)-3H-indol-1-ium-5-sulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: triphenylphosphine; carbon tetrabromide / dichloromethane / 2 h / 0 °C

3.1: sulfolane / 16 h / 110 °C / Sealed tube

With carbon tetrabromide; sodium hydride; triphenylphosphine; In tetrahydrofuran; sulfolane; dichloromethane;