4-amino-5-nitro-2-phenylthiopyrimidine

Base Information

Chemical Name:4-amino-5-nitro-2-phenylthiopyrimidine
CAS No.:124732-28-1
Molecular Formula:C₁₀H₈N₄O₂S
Molecular Weight:248.265
Hs Code.:

Synonyms:4-amino-5-nitro-2-phenylthiopyrimidine

Suppliers and Price of 4-amino-5-nitro-2-phenylthiopyrimidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-amino-5-nitro-2-phenylthiopyrimidine

Chemical Property:

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Technology Process of 4-amino-5-nitro-2-phenylthiopyrimidine

There total 1 articles about 4-amino-5-nitro-2-phenylthiopyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1920-66-7
4-amino-2-chloro-5-nitropyrimidine

: 108-98-5
thiophenol

: 124732-28-1
4-amino-5-nitro-2-phenylthiopyrimidine

Guidance literature:: With sodium ethanolate; In ethanol; for 2h; Heating;
DOI:10.1002/jhet.5570260427

Reference yield: 92.0%

: 124732-28-1
4-amino-5-nitro-2-phenylthiopyrimidine

: 124732-30-5
4,5-diamino-2-phenylthiopyrimidine

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 8h; under 2068.6 Torr; two portions of catalyst were added during the hydrogenation;
DOI:10.1002/jhet.5570260427

Reference yield:

: 124732-28-1
4-amino-5-nitro-2-phenylthiopyrimidine

: 124732-32-7
methyl 2-phenylthiopurine-8-carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / H₂ / 5percent palladium on carbon / methanol / 8 h / 2068.6 Torr / two portions of catalyst were added during the hydrogenation

2: 62 percent / N,N'-dicyclohexylcarbodiimide / acetonitrile / 6 h / Heating

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; acetonitrile;
DOI:10.1002/jhet.5570260427