Technology Process of methyl 2-phenylsulfonylpurine-8-carbamate
There total 4 articles about methyl 2-phenylsulfonylpurine-8-carbamate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dihydrogen peroxide;
In
water; acetic acid;
for 6h;
Ambient temperature;
DOI:10.1002/jhet.5570260427
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 92 percent / H2 / 5percent palladium on carbon / methanol / 8 h / 2068.6 Torr / two portions of catalyst were added during the hydrogenation
2: 62 percent / N,N'-dicyclohexylcarbodiimide / acetonitrile / 6 h / Heating
3: 93 percent / aq, hydrogen peroxide / acetic acid; H2O / 6 h / Ambient temperature
With
hydrogen; dihydrogen peroxide; dicyclohexyl-carbodiimide;
palladium on activated charcoal;
In
methanol; water; acetic acid; acetonitrile;
DOI:10.1002/jhet.5570260427
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 65 percent / sodium ethoxide / ethanol / 2 h / Heating
2: 92 percent / H2 / 5percent palladium on carbon / methanol / 8 h / 2068.6 Torr / two portions of catalyst were added during the hydrogenation
3: 62 percent / N,N'-dicyclohexylcarbodiimide / acetonitrile / 6 h / Heating
4: 93 percent / aq, hydrogen peroxide / acetic acid; H2O / 6 h / Ambient temperature
With
hydrogen; dihydrogen peroxide; sodium ethanolate; dicyclohexyl-carbodiimide;
palladium on activated charcoal;
In
methanol; ethanol; water; acetic acid; acetonitrile;
DOI:10.1002/jhet.5570260427
