methyl DL-threo-3-phenyl-2,3-O-isopropylideneglycerate

Base Information

Chemical Name:methyl DL-threo-3-phenyl-2,3-O-isopropylideneglycerate
CAS No.:81691-58-9
Molecular Formula:C₁₃H₁₆O₄
Molecular Weight:236.268
Hs Code.:

Synonyms:methyl DL-threo-3-phenyl-2,3-O-isopropylideneglycerate

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Chemical Property of methyl DL-threo-3-phenyl-2,3-O-isopropylideneglycerate

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Technology Process of methyl DL-threo-3-phenyl-2,3-O-isopropylideneglycerate

There total 3 articles about methyl DL-threo-3-phenyl-2,3-O-isopropylideneglycerate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5695-95-4,16088-08-7,55449-78-0,55449-79-1,56816-80-9,56816-81-0,60209-23-6,70094-91-6,73610-80-7
(2RS,3SR)-2,3-dihydroxy-3-phenyl-propionic acid

: 81691-58-9
methyl DL-threo-3-phenyl-2,3-O-isopropylideneglycerate

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: 9 g / ethyl orthoformate, HCl / dimethylformamide

With hydrogenchloride; orthoformic acid triethyl ester; In diethyl ether; N,N-dimethyl-formamide;

Reference yield:

: 81691-59-0
(2RS,3RS)-2,3-dihydroxy-3-phenyl-propionic acid methyl ester

: 67-64-1
acetone

: 81691-58-9
methyl DL-threo-3-phenyl-2,3-O-isopropylideneglycerate

Guidance literature:: With hydrogenchloride; orthoformic acid triethyl ester; In N,N-dimethyl-formamide;

Reference yield:

: 67-64-1
acetone

: 103-26-4,1754-62-7
methyl cinnamate

: 81691-58-9
methyl DL-threo-3-phenyl-2,3-O-isopropylideneglycerate

: (4S,5S)-2,2-Dimethyl-5-phenyl-[1,3]dioxolane-4-carboxylic acid methyl ester

Guidance literature:: With C₃₂H₃₆N₄*Fe⁽³⁺⁾*3CF₃O₃S^(1-); dihydrogen peroxide; at 60 ℃; for 24h; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/cctc.201901045