(R)-3-((4S,5R)-4-Methyl-2-oxo-5-phenyl-oxazolidine-3-carbonyl)-pentanedioic acid monomethyl ester

Base Information

Chemical Name:(R)-3-((4S,5R)-4-Methyl-2-oxo-5-phenyl-oxazolidine-3-carbonyl)-pentanedioic acid monomethyl ester
CAS No.:180293-95-2
Molecular Formula:C₁₇H₁₉NO₇
Molecular Weight:349.34
Hs Code.:

Synonyms:(R)-3-((4S,5R)-4-Methyl-2-oxo-5-phenyl-oxazolidine-3-carbonyl)-pentanedioic acid monomethyl ester

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Chemical Property of (R)-3-((4S,5R)-4-Methyl-2-oxo-5-phenyl-oxazolidine-3-carbonyl)-pentanedioic acid monomethyl ester

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Technology Process of (R)-3-((4S,5R)-4-Methyl-2-oxo-5-phenyl-oxazolidine-3-carbonyl)-pentanedioic acid monomethyl ester

There total 3 articles about (R)-3-((4S,5R)-4-Methyl-2-oxo-5-phenyl-oxazolidine-3-carbonyl)-pentanedioic acid monomethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: (R)-3-((4S,5R)-4-Methyl-2-oxo-5-phenyl-oxazolidine-3-carbonyl)-hex-5-enoic acid methyl ester

: 180293-95-2
(R)-3-((4S,5R)-4-Methyl-2-oxo-5-phenyl-oxazolidine-3-carbonyl)-pentanedioic acid monomethyl ester

Guidance literature:: With ruthenium trichloride; sodium periodate; In tetrachloromethane; water; acetonitrile;
DOI:10.1016/0040-4039(96)00816-7

Reference yield: 75.0%

: 180293-94-1
(R)-3-(3,4-Dimethoxy-benzyl)-4-((4S,5R)-4-methyl-2-oxo-5-phenyl-oxazolidin-3-yl)-4-oxo-butyric acid methyl ester

: 180293-95-2
(R)-3-((4S,5R)-4-Methyl-2-oxo-5-phenyl-oxazolidine-3-carbonyl)-pentanedioic acid monomethyl ester

Guidance literature:: With ruthenium trichloride; sodium periodate; In tetrachloromethane; water; acetonitrile;
DOI:10.1016/0040-4039(96)00816-7

Reference yield:

: 177031-11-7
(4S,5R)-3-<3-(3,4-Dimethoxyphenyl)propanoyl>-4-methyl-5-phenyl-1,3-oxazolidin-2-one

: 180293-95-2
(R)-3-((4S,5R)-4-Methyl-2-oxo-5-phenyl-oxazolidine-3-carbonyl)-pentanedioic acid monomethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / NaN(SiMe₃)2 / tetrahydrofuran / 2 h / -78 - -15 °C

2: 75 percent / RuCl₃, NaIO₄ / acetonitrile; CCl₄; H₂O

With ruthenium trichloride; sodium periodate; sodium hexamethyldisilazane; In tetrahydrofuran; tetrachloromethane; water; acetonitrile;
DOI:10.1016/0040-4039(96)00816-7