(S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionyl chloride

Base Information

• Chemical Name: (S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionyl chloride
• CAS No.: 184223-20-9
• Molecular Formula: C₁₂H₁₂ClN₃O₃S₂
• Molecular Weight: 345.831

Synonyms:(S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionyl chloride

Chemical Property of (S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionyl chloride

Chemical Property:

Purity/Quality:

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Technology Process of (S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionyl chloride

There total 2 articles about (S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionic acid (184222-95-5) → (S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionyl chloride (184223-20-9)

Guidance literature:

With thionyl chloride; In dichloromethane; Heating;

DOI:10.1021/ja961485n

Reference yield:

L-phenylalanine (63-91-2,25191-15-5,658-69-5,67675-33-6) → (S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionyl chloride (184223-20-9)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaOH

2: SOCl₂ / CH₂Cl₂ / Heating

With sodium hydroxide; thionyl chloride; In dichloromethane;

DOI:10.1021/ja961485n

Reference yield:

L-alanine methyl ester hydrochloride (2491-20-5) + (S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionyl chloride (184223-20-9) → (S)-2-[(S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionylamino]-propionic acid methyl ester

Guidance literature:

With sodium carbonate; In dichloromethane; Yield given;

DOI:10.1021/ja961485n

upstream raw materials:

(S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionic acid

L-phenylalanine

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