(S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionic acid

Base Information

Chemical Name:(S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionic acid
CAS No.:184222-95-5
Molecular Formula:C₁₂H₁₃N₃O₄S₂
Molecular Weight:327.385
Hs Code.:

Synonyms:(S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionic acid

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Chemical Property of (S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionic acid

Chemical Property:

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Technology Process of (S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionic acid

There total 1 articles about (S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 184222-90-0
5-methyl-1,3,4-thiadiazole-2-sulfonyl chloride

: 184222-95-5
(S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionic acid

Guidance literature:: With sodium hydroxide; Yield given;
DOI:10.1021/ja961485n

Reference yield:

: 184222-95-5
(S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionic acid

: 184223-20-9
(S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionyl chloride

Guidance literature:: With thionyl chloride; In dichloromethane; Heating;
DOI:10.1021/ja961485n

Reference yield:

: 184222-95-5
(S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionic acid

: (S)-2-[(S)-2-(5-Methyl-[1,3,4]thiadiazole-2-sulfonylamino)-3-phenyl-propionylamino]-propionic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / CH₂Cl₂ / Heating

2: aq. Na₂CO₃ / CH₂Cl₂

With thionyl chloride; sodium carbonate; In dichloromethane;
DOI:10.1021/ja961485n