2-(tert-butoxycarbonylamino)-3,3-dimethyl-3-[2,4-dimethyl-6-(nitrobenzene-4-sulfonyloxy)phenyl]propanol

Base Information

• Chemical Name: 2-(tert-butoxycarbonylamino)-3,3-dimethyl-3-[2,4-dimethyl-6-(nitrobenzene-4-sulfonyloxy)phenyl]propanol
• CAS No.: 1227929-86-3
• Molecular Formula: C₂₄H₃₂N₂O₈S
• Molecular Weight: 508.593
• Mol file: 1227929-86-3.mol

Synonyms:2-(tert-butoxycarbonylamino)-3,3-dimethyl-3-[2,4-dimethyl-6-(nitrobenzene-4-sulfonyloxy)phenyl]propanol

Chemical Property of 2-(tert-butoxycarbonylamino)-3,3-dimethyl-3-[2,4-dimethyl-6-(nitrobenzene-4-sulfonyloxy)phenyl]propanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2-(tert-butoxycarbonylamino)-3,3-dimethyl-3-[2,4-dimethyl-6-(nitrobenzene-4-sulfonyloxy)phenyl]propanol

There total 1 articles about 2-(tert-butoxycarbonylamino)-3,3-dimethyl-3-[2,4-dimethyl-6-(nitrobenzene-4-sulfonyloxy)phenyl]propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-(tert-butoxycarbonylamino)-3,3-dimethyl-3-[2,4-dimethyl-6-(nitrobenzene-4-sulfonyloxy)phenyl]propyl tert-butyldimethylsilyl ether (1227929-85-2) → 2-(tert-butoxycarbonylamino)-3,3-dimethyl-3-[2,4-dimethyl-6-(nitrobenzene-4-sulfonyloxy)phenyl]propanol (1227929-86-3)

Guidance literature:

With water; acetic acid; In tetrahydrofuran; Inert atmosphere;

DOI:10.1016/j.tetlet.2010.03.006

Reference yield: 91.0%

2-(tert-butoxycarbonylamino)-3,3-dimethyl-3-[2,4-dimethyl-6-(nitrobenzene-4-sulfonyloxy)phenyl]propanol (1227929-86-3) → 2-(tert-butoxycarbonylamino)-3,3-dimethyl-3-[2,4-dimethyl-6-(nitrobenzene-4-sulfonyloxy)phenyl]propanal (1227929-87-4)

Guidance literature:

With pyridinium chlorochromate; In dichloromethane; Inert atmosphere;

DOI:10.1016/j.tetlet.2010.03.006

upstream raw materials:

2-(tert-butoxycarbonylamino)-3,3-dimethyl-3-[2,4-dimethyl-6-(nitrobenzene-4-sulfonyloxy)phenyl]propyl tert-butyldimethylsilyl ether

Downstream raw materials:

2-(tert-butoxycarbonylamino)-3,3-dimethyl-3-[2,4-dimethyl-6-(nitrobenzene-4-sulfonyloxy)phenyl]propanal