S-2-bromoethyl methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)carbamothioate

Base Information

Chemical Name:S-2-bromoethyl methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)carbamothioate
CAS No.:1170733-40-0
Molecular Formula:C₂₀H₂₁BrF₃NO₂S
Molecular Weight:476.357
Hs Code.:

Synonyms:S-2-bromoethyl methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)carbamothioate

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Chemical Property of S-2-bromoethyl methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)carbamothioate

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Technology Process of S-2-bromoethyl methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)carbamothioate

There total 5 articles about S-2-bromoethyl methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)carbamothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1170733-39-7
S-2-hydroxyethyl methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)carbamothioate

: 1170733-40-0
S-2-bromoethyl methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)carbamothioate

Guidance literature:: S-2-hydroxyethyl methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)carbamothioate; With triphenylphosphine; In dichloromethane; at 0 ℃; for 0.25h; Inert atmosphere;

With carbon tetrabromide; In dichloromethane; at 0 - 25 ℃; Inert atmosphere;
DOI:10.1021/ml2000033

Reference yield:

: C₁₈H₁₇ClF₃NO₂

: 1170733-40-0
S-2-bromoethyl methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)carbamothioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 8 h / 25 °C / Inert atmosphere

2.1: triphenylphosphine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

2.2: 0 - 25 °C / Inert atmosphere

With triethylamine; triphenylphosphine; In dichloromethane;
DOI:10.1021/ml2000033

Reference yield:

: C₂₁H₂₀F₃N₃O₂

: 1170733-40-0
S-2-bromoethyl methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)carbamothioate

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 12 h / 25 °C / Inert atmosphere

2.1: triethylamine / acetonitrile / 24 h / 0 - 25 °C / Inert atmosphere

3.1: triphenylphosphine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

3.2: 0 - 25 °C / Inert atmosphere

With triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/ml2000033